4-(Phenylethinyl)triphenylmethanol

Base Information

• Chemical Name: 4-(Phenylethinyl)triphenylmethanol
• CAS No.: 13667-11-3
• Molecular Formula: C₂₇H₂₀O
• Molecular Weight: 360.455
• Mol file: 13667-11-3.mol

Synonyms:

Chemical Property of 4-(Phenylethinyl)triphenylmethanol

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 4-(Phenylethinyl)triphenylmethanol

There total 3 articles about 4-(Phenylethinyl)triphenylmethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

benzophenone (119-61-9) + 1-bromo-4-phenylethynylbenzene (13667-12-4) → 4-(Phenylethinyl)triphenylmethanol (13667-11-3)

Guidance literature:

Multistep reaction; (i) Mg, BrCH₂CH₂Br, (ii) /BRN= 1238185/;

DOI:10.1007/BF00907137

Reference yield:

bromobenzene (108-86-1,52753-63-6) → 4-(Phenylethinyl)triphenylmethanol (13667-11-3)

Guidance literature:

Multi-step reaction with 3 steps

1: AlCl₃

2: (i) PCl₃, (ii) KOH

3: (i) Mg, BrCH₂CH₂Br, (ii) /BRN= 1238185/

With aluminium trichloride;

DOI:10.1007/BF00907137

Reference yield:

1-(4-bromophenyl)-2-phenyl-ethan-1-one (2001-29-8) → 4-(Phenylethinyl)triphenylmethanol (13667-11-3)

Guidance literature:

Multi-step reaction with 2 steps

1: (i) PCl₃, (ii) KOH

2: (i) Mg, BrCH₂CH₂Br, (ii) /BRN= 1238185/

DOI:10.1007/BF00907137

upstream raw materials:

benzophenone

1-bromo-4-phenylethynylbenzene

bromobenzene

1-(4-bromophenyl)-2-phenyl-ethan-1-one

Downstream raw materials:

1-(Chloro-diphenyl-methyl)-4-phenylethynyl-benzene