C₁₈H₂₈O₈

Base Information

• Chemical Name: C₁₈H₂₈O₈
• CAS No.: 1451984-60-3
• Molecular Formula: C₁₈H₂₈O₈
• Molecular Weight: 372.416
• Mol file: 1451984-60-3.mol

Synonyms:

Chemical Property of C₁₈H₂₈O₈

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₈H₂₈O₈

There total 1 articles about C₁₈H₂₈O₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

tetraethylene glycol monomethyl ether (23783-42-8,95507-80-5) → C18H28O8 (1451984-60-3)

Guidance literature:

Multi-step reaction with 2 steps

1: sodium hydroxide / tetrahydrofuran; water / 8 h / 0 °C / Inert atmosphere

2: caesium carbonate / N,N-dimethyl-formamide / 0.33 h / 160 °C / Microwave irradiation; Inert atmosphere

With caesium carbonate; sodium hydroxide; In tetrahydrofuran; water; N,N-dimethyl-formamide;

DOI:10.1021/jm400665c

Reference yield:

Methyl azidoacetate (1816-92-8) + C18H28O8 (1451984-60-3) → C21H31N3O9

Guidance literature:

With sodium methylate; In methanol; at 0 ℃; for 4h; Inert atmosphere;

DOI:10.1021/jm400665c

upstream raw materials:

tetraethylene glycol monomethyl ether