(2,4,10-Trioxaadamant-3-yl)trimethylammonium-iodid

Base Information

Chemical Name:(2,4,10-Trioxaadamant-3-yl)trimethylammonium-iodid
CAS No.:93563-99-6
Molecular Formula:C₁₀H₁₈NO₃*I
Molecular Weight:327.162
Hs Code.:

Synonyms:

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Chemical Property of (2,4,10-Trioxaadamant-3-yl)trimethylammonium-iodid

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Technology Process of (2,4,10-Trioxaadamant-3-yl)trimethylammonium-iodid

There total 6 articles about (2,4,10-Trioxaadamant-3-yl)trimethylammonium-iodid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 93563-91-8
3-Amino-2,4,10-trioxaadamantan

: 74-88-4
methyl iodide

: 93563-99-6
(2,4,10-Trioxaadamant-3-yl)trimethylammonium-iodid

Guidance literature:: With sodium carbonate; In acetonitrile; for 1h; Heating;

Reference yield:

: 108-73-6
3,5-dihydroxyphenol

: 93563-99-6
(2,4,10-Trioxaadamant-3-yl)trimethylammonium-iodid

Guidance literature:: Multi-step reaction with 6 steps

1: 60 percent / H₂ / Raney-Ni / ethanol; H₂O / 48 h / 112509 - 150012 Torr / Ambient temperature

2: 91 percent / Et₂O*BF₃ / CH₂Cl₂ / 1.) 8 - 12 h, reflux; 2.) 24 h at room temp.

3: 91 percent / NH₃-gas / methanol / Heating

4: 82 percent / PhI(OAc)2 / pyridine / 4 h

5: 66 percent / 2N NaOH / 0.17 h / Heating

6: 79 percent / Na₂CO₃ / acetonitrile / 1 h / Heating

With sodium hydroxide; [bis(acetoxy)iodo]benzene; boron trifluoride diethyl etherate; ammonia; hydrogen; sodium carbonate; nickel; In pyridine; methanol; ethanol; dichloromethane; water; acetonitrile;

Reference yield:

: 50409-12-6,13314-30-2
cis,cis-1,3,5-trihydroxycyclohexane

: 93563-99-6
(2,4,10-Trioxaadamant-3-yl)trimethylammonium-iodid

Guidance literature:: Multi-step reaction with 5 steps

1: 91 percent / Et₂O*BF₃ / CH₂Cl₂ / 1.) 8 - 12 h, reflux; 2.) 24 h at room temp.

2: 91 percent / NH₃-gas / methanol / Heating

3: 82 percent / PhI(OAc)2 / pyridine / 4 h

4: 66 percent / 2N NaOH / 0.17 h / Heating

5: 79 percent / Na₂CO₃ / acetonitrile / 1 h / Heating

With sodium hydroxide; [bis(acetoxy)iodo]benzene; boron trifluoride diethyl etherate; ammonia; sodium carbonate; In pyridine; methanol; dichloromethane; acetonitrile;