trans-[PdCl₂(AsMe₂Ph)2]

Base Information

• Chemical Name: trans-[PdCl₂(AsMe₂Ph)2]
• CAS No.: 64043-85-2
• Molecular Formula: C₁₆H₂₂As₂Cl₂Pd
• Molecular Weight: 541.52

Synonyms:

Chemical Property of trans-[PdCl₂(AsMe₂Ph)2]

Chemical Property:

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Technology Process of trans-[PdCl₂(AsMe₂Ph)2]

There total 1 articles about trans-[PdCl₂(AsMe₂Ph)2] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

dimethylphenylarsine (696-26-4) + palladium dichloride → [PdCl2(As(CH3)2(C6H5))2] (64043-85-2,15130-24-2,40791-50-2)

Guidance literature:

With HCl; In methanol; water; PdCl2 dissolved in aq. HCl by gentle warming, added EtOH and ligand; ppt. sepd., recrystd. from CH2Cl2 by addn. of Et2O;

Reference yield: 98.0%

silver(I) hexafluorophosphate (26042-63-7) + [PdCl2(As(CH3)2(C6H5))2] (64043-85-2,15130-24-2,40791-50-2) + cyclopenta-1,3-diene (542-92-7,25568-84-7,7313-32-8) → [Pd(C5H5)(As(CH3)2(C6H5))2](1+)*PF6(1-)*0.5(CH3)2CO=[Pd(C5H5)(As(CH3)2(C6H5))2]PF6*0.5(CH3)2CO

Guidance literature:

With acetone; In acetone; byproducts: AgCl; to suspn. of Pd complex in acetone added soln. of AgPF6 in acetone, AgCl filtered, added C5H6; pptd. by addn. of Et2O, recrystd. from acetone by addn. of Et2O; elem. anal.;

Reference yield:

trans-[PdCl2(AsMe2Ph)2] (40791-50-2,15130-24-2,64043-85-2) → [PdCl4(As(CH3)2(C6H5))2] (83970-97-2)

Guidance literature:

With Cl₂; In tetrachloromethane; small excess of Cl2 slowly bubbled through stirred suspn. of Pd complexin dry CCl4, stirred for 30 min; filtered, but not pumped dry, dried in vac.; elem. anal.;

DOI:10.1039/DT9820001895

upstream raw materials:

dimethylphenylarsine

Downstream raw materials:

[PdCl₄(As(CH₃)2(C₆H₅))2]

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