Fe(C₅H₄)2C₆H₅GeCl

Base Information

Chemical Name:Fe(C₅H₄)2C₆H₅GeCl
CAS No.:403817-49-2
Molecular Formula:C₁₆H₁₃ClFeGe
Molecular Weight:369.169
Hs Code.:

Fe(C<sub>5</sub>H<sub>4</sub>)2C<sub>6</sub>H<sub>5</sub>GeCl

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Fe(C₅H₄)2C₆H₅GeCl

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Technology Process of Fe(C₅H₄)2C₆H₅GeCl

There total 1 articles about Fe(C₅H₄)2C₆H₅GeCl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 102-54-5,55404-68-7
ferrocene

: 1074-29-9
trichlorophenylgermane

: 403817-49-2
Fe(C₅H₄)2C₆H₅GeCl

Guidance literature:: With n-BuLi; TMEDA; In hexane; to soln. of Fe-complex, TMEDA in hexane was added n-BuLi, stirred for 18h, washed with hexane, ether was added, stirred at -78°C, ligand was added over 10 min, warmed to room temp., stirred overnight under Ar; filtered, solvent was removed in vacuo, crystd. from hexane; elem. anal.;
DOI:10.1016/S0022-328X(01)00962-7

Reference yield: 89.0%

: 7647-01-0,15364-23-5
hydrogenchloride

: 403817-49-2
Fe(C₅H₄)2C₆H₅GeCl

: 403817-43-6
ferrocenyl(phenyl)dichlorogermane

Guidance literature:: In diethyl ether; hexane; to soln. of Fe-complex in hexane was added dropwise at room temp. HCl inether, stirred for 15 min under Ar; filtered, solvent was removed in vacuo; elem. anal.;
DOI:10.1016/S0022-328X(01)00962-7