C₄₆H₄₈N₂O₁₅

Base Information

Chemical Name:C₄₆H₄₈N₂O₁₅
CAS No.:1429637-90-0
Molecular Formula:C₄₆H₄₈N₂O₁₅
Molecular Weight:868.892
Hs Code.:

C<sub>46</sub>H<sub>48</sub>N<sub>2</sub>O<sub>15</sub>

Synonyms:

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Chemical Property of C₄₆H₄₈N₂O₁₅

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Technology Process of C₄₆H₄₈N₂O₁₅

There total 19 articles about C₄₆H₄₈N₂O₁₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 73-32-5,959215-79-3,18875-42-8
L-isoleucine

: 1429637-90-0
C₄₆H₄₈N₂O₁₅

: 1429637-91-1
C₄₆H₄₈N₂O₁₅

: 1429637-92-2
C₄₆H₄₈N₂O₁₅

: 1429637-93-3
C₄₆H₄₈N₂O₁₅

Guidance literature:: Multi-step reaction with 7 steps

1.1: ethylene glycol / 18 h / 200 °C / Inert atmosphere

2.1: trichlorophosphate / 12 h / 100 °C / Inert atmosphere

3.1: trifluoroacetic acid; dihydrogen peroxide / 3 h / 50 °C / Inert atmosphere

4.1: sodium t-butanolate / tetrahydrofuran / 12 h / 23 °C / Inert atmosphere

5.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h / 23 °C / Inert atmosphere

5.2: 2 h / 23 °C / Inert atmosphere

6.1: trifluoroacetic acid / dichloromethane / 0.5 h / 23 °C / Inert atmosphere

7.1: chloroform-d1 / 1 h / 23 °C / Inert atmosphere

With tetrabutyl ammonium fluoride; dihydrogen peroxide; trifluoroacetic acid; sodium t-butanolate; trichlorophosphate; In tetrahydrofuran; chloroform-d1; dichloromethane; ethylene glycol; 7.1: |Diels-Alder Cycloaddition;
DOI:10.1021/ol400709f

Reference yield:

: 1264728-58-6
3,6-di((S)-sec-butyl)piperazine-2,5-dione

: 1429637-90-0
C₄₆H₄₈N₂O₁₅

: 1429637-91-1
C₄₆H₄₈N₂O₁₅

: 1429637-92-2
C₄₆H₄₈N₂O₁₅

: 1429637-93-3
C₄₆H₄₈N₂O₁₅

Guidance literature:: Multi-step reaction with 6 steps

1.1: trichlorophosphate / 12 h / 100 °C / Inert atmosphere

2.1: trifluoroacetic acid; dihydrogen peroxide / 3 h / 50 °C / Inert atmosphere

3.1: sodium t-butanolate / tetrahydrofuran / 12 h / 23 °C / Inert atmosphere

4.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h / 23 °C / Inert atmosphere

4.2: 2 h / 23 °C / Inert atmosphere

5.1: trifluoroacetic acid / dichloromethane / 0.5 h / 23 °C / Inert atmosphere

6.1: chloroform-d1 / 1 h / 23 °C / Inert atmosphere

With tetrabutyl ammonium fluoride; dihydrogen peroxide; trifluoroacetic acid; sodium t-butanolate; trichlorophosphate; In tetrahydrofuran; chloroform-d1; dichloromethane; 6.1: |Diels-Alder Cycloaddition;
DOI:10.1021/ol400709f

Reference yield:

: 1429637-78-4
2,5-di((S)-sec-butyl)-3-chloropyrazine

: 1429637-90-0
C₄₆H₄₈N₂O₁₅

: 1429637-91-1
C₄₆H₄₈N₂O₁₅

: 1429637-92-2
C₄₆H₄₈N₂O₁₅

: 1429637-93-3
C₄₆H₄₈N₂O₁₅

Guidance literature:: Multi-step reaction with 6 steps

1.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 4 h / 40 °C / Inert atmosphere

1.2: 2 h / 100 °C / Inert atmosphere

2.1: trifluoroacetic acid; dihydrogen peroxide / 3 h / 50 °C / Inert atmosphere

3.1: sodium t-butanolate / tetrahydrofuran / 12 h / 23 °C / Inert atmosphere

4.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h / 23 °C / Inert atmosphere

4.2: 2 h / 23 °C / Inert atmosphere

5.1: trifluoroacetic acid / dichloromethane / 0.5 h / 23 °C / Inert atmosphere

6.1: chloroform-d1 / 1 h / 23 °C / Inert atmosphere

With tetrabutyl ammonium fluoride; dihydrogen peroxide; 3-chloro-benzenecarboperoxoic acid; trifluoroacetic acid; sodium t-butanolate; In tetrahydrofuran; chloroform-d1; dichloromethane; 6.1: |Diels-Alder Cycloaddition;
DOI:10.1021/ol400709f