bis(6-mercapto-9-methylpurine)bis(triphenylphosphine)ruthenium(II)chloride * 1.5 H₂O

Base Information

• Chemical Name: bis(6-mercapto-9-methylpurine)bis(triphenylphosphine)ruthenium(II)chloride * 1.5 H₂O
• CAS No.: 98218-99-6
• Molecular Formula: C₄₈H₄₂N₈P₂RuS₂*2Cl*H₂O
• Molecular Weight: 1055.99

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Chemical Property of bis(6-mercapto-9-methylpurine)bis(triphenylphosphine)ruthenium(II)chloride * 1.5 H₂O

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Technology Process of bis(6-mercapto-9-methylpurine)bis(triphenylphosphine)ruthenium(II)chloride * 1.5 H₂O

There total 1 articles about bis(6-mercapto-9-methylpurine)bis(triphenylphosphine)ruthenium(II)chloride * 1.5 H₂O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

tris(triphenylphosphine)ruthenium(II) chloride (15529-49-4,41756-81-4) + 9-methyl-1,9-dihydro-6H-purine-6-thione (1006-20-8) → bis(6-mercapto-9-methylpurine)bis(triphenylphosphine)ruthenium(II)chloride * 1.5 H2O (98218-99-6)

Guidance literature:

In ethanol; flushing a suspension of 2 mmol purine in ethanol with N2 for 0.5 h; addn. of 1 mmol (RuCl2(P(C6H5)3)3); refluxing and stirring of the mixture for 1 h under N2; cooling to ambient temp.;; pptn.; washed twice with cold ethanol; recrystd. twice from ethanol; washed twice with ethanol and ether; dried in vacuum for 8 h; elem. anal.;;

upstream raw materials:

tris(triphenylphosphine)ruthenium(II) chloride

9-methyl-1,9-dihydro-6H-purine-6-thione

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