Technology Process of 2-(Triphenylstannyl)benzothiazole
There total 1 articles about 2-(Triphenylstannyl)benzothiazole which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
n-Buli;
In
tetrahydrofuran; diethyl ether; hexane;
under N2, addn. of soln. of n-Buli in hexane to soln. of benzothiazole in THF during 1 h, stirring at -10 ° C for 1 h, addn. of soln. of triphenyltin chloride in Et2O during 1 h, warming up to room temp.; filtration, evapn., distn., elem. anal.;
DOI:10.1016/0022-328X(89)87167-0
- Guidance literature:
-
With
iodine;
In
tetrachloromethane;
under N2, addn. of soln. of iodine in CCl4 over a period of 1 h to a soln. of Ph3SnBox in petrol ether at room temp., stirring for 1 h; evapn., redissolving in hot petrol ether, filtration, white prisms were obtained by coolimg, elem. anal.;
DOI:10.1016/0022-328X(89)87167-0