C₆H₅CHCHCOHFe(CO)3

Base Information

Chemical Name:C₆H₅CHCHCOHFe(CO)3
CAS No.:38704-79-9
Molecular Formula:C₁₂H₈FeO₄
Molecular Weight:272.04
Hs Code.:

C<sub>6</sub>H<sub>5</sub>CHCHCOHFe(CO)3

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₆H₅CHCHCOHFe(CO)3

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Technology Process of C₆H₅CHCHCOHFe(CO)3

There total 1 articles about C₆H₅CHCHCOHFe(CO)3 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: 15321-51-4
diiron nonacarbonyl

: 104-55-2
3-phenyl-propenal

: 38704-79-9,142435-19-6,38720-33-1,142435-18-5
C₆H₅CHCHCOHFe(CO)3

Guidance literature:: In diethyl ether; 2 equivalents of Fe compd. and carbonyl compd. were heated in ether for 15 - 18 h;
DOI:10.1039/c39890000021

Reference yield: 5.0%

: 38704-79-9,142435-19-6,38720-33-1,142435-18-5
C₆H₅CHCHCOHFe(CO)3

: 507-19-7
t-butyl bromide

: 917-54-4
methyllithium

: tricarbonyl(η4-1,6-diphenylhexa-1,3,5-triene)iron

: 1720-32-7,17329-15-6,38557-34-5,38557-35-6,118493-17-7,125341-41-5
1,6-diphenyl-1,3,5-hexatriene

Guidance literature:: In tetrahydrofuran; (CO); -78 °C; stirring for 2 h, addn. of tert.-butyl bromide, stirring for 0.5 h, removal of cooling bath, stirring for 1 h.; chromy. (SiO2); ethyl acetate-Et2O, 1:49;

Reference yield: 5.0%

: 38704-79-9,142435-19-6,38720-33-1,142435-18-5
C₆H₅CHCHCOHFe(CO)3

: 917-54-4
methyllithium

: C₆H₅CHCHCHCOFe(CO)3

: tricarbonyl(η4-1,6-diphenylhexa-1,3,5-triene)iron

Guidance literature:: With C(CH₃)3Br; In tetrahydrofuran; carbonyl compd. and MeLi was stirred at -78°C in THF for 2 h under CO atmosphere (1,1 atm.), then tBuBr was added and stirred for further 0,5 h at the same temp., mixt. was then allowed to warm up to room temp. over 1 h under CO; soln. filtered through alumina and chromd.;
DOI:10.1039/c39890000021