3,4-diphenyl-1H-pyrrole-2,5-dicarboxylic acid diferrocenylmethyl-amide

Base Information

Chemical Name:3,4-diphenyl-1H-pyrrole-2,5-dicarboxylic acid diferrocenylmethyl-amide
CAS No.:475148-10-8
Molecular Formula:C₄₀H₃₅Fe₂N₃O₂
Molecular Weight:701.431
Hs Code.:

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Chemical Property of 3,4-diphenyl-1H-pyrrole-2,5-dicarboxylic acid diferrocenylmethyl-amide

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Technology Process of 3,4-diphenyl-1H-pyrrole-2,5-dicarboxylic acid diferrocenylmethyl-amide

There total 2 articles about 3,4-diphenyl-1H-pyrrole-2,5-dicarboxylic acid diferrocenylmethyl-amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 31.0%

: 1273-82-1
aminoferrocene

: 365214-51-3
3,4-diphenylpyrrole-2,5-dicarboxylic acid chloride

: 475148-10-8
3,4-diphenyl-1H-pyrrole-2,5-dicarboxylic acid diferrocenylmethyl-amide

Guidance literature:: With Et₃N; 4-N,N-dimethylaminopyridine; In dichloromethane; stirring soln. of diphenyl-pyrrole-dicarbonyl dichloride in dry CH2Cl2 under N2, addn. of Et3N, catalytic amt. of dimethylaminopyridine, and slight excess of Fe-compd., stirring under N2 overnight; solvent was removed in vac., residue was redissolved in MeCN, ppt. was sepd., washed 3 times with MeCN and H2O, resp., dried in high vac. for 2 h, chromy. (silica/ CH2Cl2-2% MeOH);
DOI:10.1039/b202989h

Reference yield: 31.0%

: (aminomethyl)ferrocene

: 365214-51-3
3,4-diphenylpyrrole-2,5-dicarboxylic acid chloride

: 475148-10-8
3,4-diphenyl-1H-pyrrole-2,5-dicarboxylic acid diferrocenylmethyl-amide

Guidance literature:: With triethylamine; DMAP (catalyst); In dichloromethane; N2, stirred overnight; solvent removed (vac.), dissolved (CH3CN), ppt. filtered, washed (acetonitrile, water), dried (vac., 2 h), chromy. (TLC, silica, CH2Cl2/methanol); elem. anal.;
DOI:10.1016/S0277-5387(02)01401-8