(3R,4S)-1-(benzyloxy)-4-methylhept-6-en-3-ol

Base Information

Chemical Name:(3R,4S)-1-(benzyloxy)-4-methylhept-6-en-3-ol
CAS No.:1299293-78-9
Molecular Formula:C₁₅H₂₂O₂
Molecular Weight:234.338
Hs Code.:

Synonyms:

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Chemical Property of (3R,4S)-1-(benzyloxy)-4-methylhept-6-en-3-ol

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Technology Process of (3R,4S)-1-(benzyloxy)-4-methylhept-6-en-3-ol

There total 4 articles about (3R,4S)-1-(benzyloxy)-4-methylhept-6-en-3-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 19790-60-4
3-Benzyloxypropanal

: 1299293-78-9
(3R,4S)-1-(benzyloxy)-4-methylhept-6-en-3-ol

Guidance literature:: Multi-step reaction with 3 steps

1.1: diethylzinc; palladium diacetate; triphenylphosphine / tetrahydrofuran / -80 - -20 °C

2.1: 2-methyl-but-2-ene; dimethylsulfide borane complex / tetrahydrofuran / 0 - 20 °C

2.2: 0 - 20 °C

3.1: potassium tert-butylate / tetrahydrofuran / 0.5 h / 0 °C

3.2: 0 - 20 °C

With 2-methyl-but-2-ene; dimethylsulfide borane complex; potassium tert-butylate; diethylzinc; palladium diacetate; triphenylphosphine; In tetrahydrofuran; 1.1: Marshall-Tamaru reaction / 3.1: Wittig reaction / 3.2: Wittig reaction;
DOI:10.1055/s-0030-1259287

Reference yield:

: 1299293-76-7
(3R,4S)-1-(benzyloxy)-4-methylhex-5-yn-3-ol

: 1299293-78-9
(3R,4S)-1-(benzyloxy)-4-methylhept-6-en-3-ol

Guidance literature:: Multi-step reaction with 2 steps

1.1: 2-methyl-but-2-ene; dimethylsulfide borane complex / tetrahydrofuran / 0 - 20 °C

1.2: 0 - 20 °C

2.1: potassium tert-butylate / tetrahydrofuran / 0.5 h / 0 °C

2.2: 0 - 20 °C

With 2-methyl-but-2-ene; dimethylsulfide borane complex; potassium tert-butylate; In tetrahydrofuran; 2.1: Wittig reaction / 2.2: Wittig reaction;
DOI:10.1055/s-0030-1259287

Reference yield:

: 100-39-0
benzyl bromide

: 1299293-78-9
(3R,4S)-1-(benzyloxy)-4-methylhept-6-en-3-ol

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium hydride / tetrahydrofuran / 20 °C

1.2: 20 °C

2.1: oxalyl dichloride; dimethyl sulfoxide; triethylamine / dichloromethane / -80 - 20 °C

3.1: diethylzinc; palladium diacetate; triphenylphosphine / tetrahydrofuran / -80 - -20 °C

4.1: 2-methyl-but-2-ene; dimethylsulfide borane complex / tetrahydrofuran / 0 - 20 °C

4.2: 0 - 20 °C

5.1: potassium tert-butylate / tetrahydrofuran / 0.5 h / 0 °C

5.2: 0 - 20 °C

With 2-methyl-but-2-ene; oxalyl dichloride; dimethylsulfide borane complex; potassium tert-butylate; diethylzinc; palladium diacetate; sodium hydride; dimethyl sulfoxide; triethylamine; triphenylphosphine; In tetrahydrofuran; dichloromethane; 3.1: Marshall-Tamaru reaction / 5.1: Wittig reaction / 5.2: Wittig reaction;
DOI:10.1055/s-0030-1259287