[(ClC₆H₃CHN(CH(CH₂C₆H₅)(COOC₂H₅)))PdCl]2

Base Information

• Chemical Name: [(ClC₆H₃CHN(CH(CH₂C₆H₅)(COOC₂H₅)))PdCl]2
• CAS No.: 511546-88-6
• Molecular Formula: C₃₆H₃₄Cl₄N₂O₄Pd₂
• Molecular Weight: 913.329

Synonyms:

Chemical Property of [(ClC₆H₃CHN(CH(CH₂C₆H₅)(COOC₂H₅)))PdCl]2

Chemical Property:

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Technology Process of [(ClC₆H₃CHN(CH(CH₂C₆H₅)(COOC₂H₅)))PdCl]2

There total 1 articles about [(ClC₆H₃CHN(CH(CH₂C₆H₅)(COOC₂H₅)))PdCl]2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

palladium diacetate (3375-31-3) + lithium chloride + 4-ClC6H4CH=NCH(CH2Ph)COOEt → [(ClC6H3CHN(CH(CH2C6H5)(COOC2H5)))PdCl]2 (511546-88-6)

Guidance literature:

In acetic acid; acetone; (N2); stirred suspn. of Pd(OAc)2 in AcOH was treated with ligand for 3 hat 70°C; concd. (vac.); residue dissolved in acetone and treated with LiCl for 30 min at room temp.; concd. (vac.); chromd. (SiO2, CHCl3/acetone, 100/4); elem. anal.;

DOI:10.1016/S0022-328X(02)01928-9

Reference yield: 75.0%

[(ClC6H3CHN(CH(CH2C6H5)(COOC2H5)))PdCl]2 (511546-88-6) + triphenylphosphine (603-35-0) → [(ClC6H3CHN(CH(CH2C6H5)(COOC2H5)))PdCl(P(C6H5)3)] (511546-94-4)

Guidance literature:

In acetone; suspn. of Pd complex in acetone was treated with PPh3; mixt. was stirredat room temp. for 30 min; concd. (vac.); washed (Et2O); elem. anal.;

DOI:10.1016/S0022-328X(02)01928-9

Reference yield:

perdeuteriopyridine (7291-22-7) + [(ClC6H3CHN(CH(CH2C6H5)(COOC2H5)))PdCl]2 (511546-88-6) → [(ClC6H3CHN(CH(CH2C6H5)(COOC2H5)))PdCl(NC5D5)]

Guidance literature:

In chloroform-d1; few drops of pyridine-d5 was added to soln. of Pd complex in CDCl3; not isolated; NMR monitoring;

DOI:10.1016/S0022-328X(02)01928-9

upstream raw materials:

palladium diacetate

Downstream raw materials:

[(ClC₆H₃CHN(CH(CH₂C₆H₅)(COOC₂H₅)))PdCl(P(C₆H₅)3)]

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