MoCl₂(N₂(CH₃)C₆H₅)(S(CH₂CH₂S)2)

Base Information

• Chemical Name: MoCl₂(N₂(CH₃)C₆H₅)(S(CH₂CH₂S)2)
• CAS No.: 642988-50-9
• Molecular Formula: C₁₁H₁₆Cl₂MoN₂S₃
• Molecular Weight: 439.305
• Mol file: 642988-50-9.mol

Synonyms:

Chemical Property of MoCl₂(N₂(CH₃)C₆H₅)(S(CH₂CH₂S)2)

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of MoCl₂(N₂(CH₃)C₆H₅)(S(CH₂CH₂S)2)

There total 1 articles about MoCl₂(N₂(CH₃)C₆H₅)(S(CH₂CH₂S)2) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

chloro-trimethyl-silane (75-77-4) + MoO(N2(CH3)C6H5)(S(CH2CH2S)2) → MoCl2(N2(CH3)C6H5)(S(CH2CH2S)2) (642988-50-9)

Guidance literature:

In tetrahydrofuran; ligand was added to soln. of Mo-complex in THF, stirred for 24 h under N2; filtered, washed with THF, dried under vac.;

DOI:10.1016/S0020-1693(03)00051-3

Reference yield: 61.0%

MoCl2(N2(CH3)C6H5)(S(CH2CH2S)2) (642988-50-9) + disodium 3,6-di-tert-butyl-o-catecholate → Mo(C6H2O2(C4H9)2)(N2CH3C6H5)(S(CH2CH2S)2) (642988-51-0)

Guidance literature:

In tetrahydrofuran; ligand in THF was added to suspn. of Mo-complex in THF, stirred for 24 hunder N2; solvent was removed in vacuo, solidified with n-hexane, filtered, washedwith n-hexane, extd. with CH2Cl2, layered with n-hexane, allowed to sta nd for 2 d at room temp.; elem. anal.;

DOI:10.1016/S0020-1693(03)00051-3

upstream raw materials:

chloro-trimethyl-silane

Downstream raw materials:

Mo(C₆H₂O₂(C₄H₉)2)(N₂CH₃C₆H₅)(S(CH₂CH₂S)2)