1,2-Cyclopentanediol, 3-chloro-4-(phenylsulfonyl)-

Base Information

Chemical Name:1,2-Cyclopentanediol, 3-chloro-4-(phenylsulfonyl)-
CAS No.:105064-19-5
Molecular Formula:C11H13ClO4S
Molecular Weight:276.741
Hs Code.:
Mol file:105064-19-5.mol

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,2-Cyclopentanediol, 3-chloro-4-(phenylsulfonyl)-

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 1,2-Cyclopentanediol, 3-chloro-4-(phenylsulfonyl)-

There total 4 articles about 1,2-Cyclopentanediol, 3-chloro-4-(phenylsulfonyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.7%

: 60034-64-2
trans-4-chloro-5-(phenylsulfonyl)-2-cyclopentene

: 105064-19-5
trans-4-chloro-cis-2,3-dihydroxy-5-(phenylsulfonyl)-2-cyclopentane

Guidance literature:: With osmium(VIII) oxide; di-tert-butyl peroxide; tetraethylammonium acetate; sodium acetate; In water; acetone; for 72h; Ambient temperature;
DOI:10.1021/jo00380a019

Reference yield:

: 60034-57-3
1-chloro-2-(phenylsulfenyl)cyclopenta-2,4-diene

: 105064-19-5
trans-4-chloro-cis-2,3-dihydroxy-5-(phenylsulfonyl)-2-cyclopentane

Guidance literature:: Multi-step reaction with 2 steps

1: m-chloroperoxybenzoic acid (MCPBA) / CH₂Cl₂ / 16 h / 25 °C

2: 81.7 percent / tetraethylammonium acetate, sodium acetate, 90percent tert-butyl peroxide, osmium tetroxide / H₂O; acetone / 72 h / Ambient temperature

With osmium(VIII) oxide; di-tert-butyl peroxide; tetraethylammonium acetate; sodium acetate; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; water; acetone;
DOI:10.1021/jo00380a019

Reference yield:

: 108-98-5
thiophenol

: 105064-19-5
trans-4-chloro-cis-2,3-dihydroxy-5-(phenylsulfonyl)-2-cyclopentane

Guidance literature:: Multi-step reaction with 4 steps

1: N-chlorosuccinimide / CH₂Cl₂ / 0.5 h / 25 °C

2: CH₂Cl₂ / -78 - -50 °C

3: m-chloroperoxybenzoic acid (MCPBA) / CH₂Cl₂ / 16 h / 25 °C

4: 81.7 percent / tetraethylammonium acetate, sodium acetate, 90percent tert-butyl peroxide, osmium tetroxide / H₂O; acetone / 72 h / Ambient temperature

With N-chloro-succinimide; osmium(VIII) oxide; di-tert-butyl peroxide; tetraethylammonium acetate; sodium acetate; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; water; acetone;
DOI:10.1021/jo00380a019