C₁₃H₁₈O₂

Base Information

Chemical Name:C₁₃H₁₈O₂
CAS No.:1402922-15-9
Molecular Formula:C₁₃H₁₈O₂
Molecular Weight:206.285
Hs Code.:

C<sub>13</sub>H<sub>18</sub>O<sub>2</sub>

Synonyms:

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Chemical Property of C₁₃H₁₈O₂

Chemical Property:

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Technology Process of C₁₃H₁₈O₂

There total 5 articles about C₁₃H₁₈O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₀H₁₄O

: 79-03-8
propionyl chloride

: 1402922-15-9
C₁₃H₁₈O₂

Guidance literature:: With C₂₃H₃₂N₂O₂Si; lithium perchlorate; In diethyl ether; dichloromethane; at -40 ℃; for 19h; enantioselective reaction; Inert atmosphere;
DOI:10.1002/anie.201202643

Reference yield:

: 1402922-12-6
C₂₀H₂₃NO₃

: 1402922-15-9
C₁₃H₁₈O₂

Guidance literature:: Multi-step reaction with 4 steps

1.1: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / toluene / 2 h / 40 °C / Inert atmosphere

2.1: lithium borohydride / tetrahydrofuran; methanol / 2 h / 0 °C / Inert atmosphere

3.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.25 h / -78 °C / Inert atmosphere

3.2: 1.5 h / -78 - 0 °C / Inert atmosphere

4.1: C₂₃H₃₂N₂O₂Si; lithium perchlorate / diethyl ether; dichloromethane / 19 h / -40 °C / Inert atmosphere

With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; lithium borohydride; oxalyl dichloride; C₂₃H₃₂N₂O₂Si; lithium perchlorate; dimethyl sulfoxide; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; toluene; 3.1: Swern oxidation / 3.2: Swern oxidation;
DOI:10.1002/anie.201202643

Reference yield:

: 1402922-11-5
C₁₇H₁₉NO₃

: 1402922-15-9
C₁₃H₁₈O₂

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium hexamethyldisilazane / tetrahydrofuran / -78 °C / Inert atmosphere

1.2: -40 °C / Inert atmosphere

2.1: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / toluene / 2 h / 40 °C / Inert atmosphere

3.1: lithium borohydride / tetrahydrofuran; methanol / 2 h / 0 °C / Inert atmosphere

4.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.25 h / -78 °C / Inert atmosphere

4.2: 1.5 h / -78 - 0 °C / Inert atmosphere

5.1: C₂₃H₃₂N₂O₂Si; lithium perchlorate / diethyl ether; dichloromethane / 19 h / -40 °C / Inert atmosphere

With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; lithium borohydride; oxalyl dichloride; C₂₃H₃₂N₂O₂Si; lithium perchlorate; sodium hexamethyldisilazane; dimethyl sulfoxide; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; toluene; 4.1: Swern oxidation / 4.2: Swern oxidation;
DOI:10.1002/anie.201202643