Technology Process of N4-acetyl-2',5'-di-O-p-chlorobenzoyl-3'-deoxycytidine
There total 1 articles about N4-acetyl-2',5'-di-O-p-chlorobenzoyl-3'-deoxycytidine which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 4.0 g / H2SO4 / acetic acid; acetic anhydride / 2 h / Ambient temperature
2: stannic chloride / acetonitrile / Ambient temperature
With
sulfuric acid; tin(IV) chloride;
In
acetic anhydride; acetic acid; acetonitrile;
DOI:10.1248/cpb.30.2223
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 980 mg / sodium methoxide / methanol / 5 h / Ambient temperature
2: 74 percent / tetrachloropyrophosphate / acetonitrile / Ambient temperature
With
sodium methylate;
In
methanol; acetonitrile;
DOI:10.1248/cpb.30.2223
- Guidance literature:
-
With
sodium methylate;
In
methanol;
for 5h;
Ambient temperature;
DOI:10.1248/cpb.30.2223
