Technology Process of C32H35ClN2O2S
There total 10 articles about C32H35ClN2O2S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 6 steps
1: potassium carbonate / acetone / Reflux
2: sodium hydrogen sulfide; magnesium chloride / N,N-dimethyl-formamide / 20 °C
3: ethanol / Reflux
4: boron tribromide / dichloromethane / -78 °C
5: potassium carbonate / acetonitrile / Reflux
6: potassium carbonate / acetonitrile / Reflux
With
sodium hydrogen sulfide; boron tribromide; potassium carbonate; magnesium chloride;
In
ethanol; dichloromethane; N,N-dimethyl-formamide; acetone; acetonitrile;
DOI:10.1016/j.bmcl.2012.10.022
- Guidance literature:
-
Multi-step reaction with 4 steps
1: ethanol / Reflux
2: boron tribromide / dichloromethane / -78 °C
3: potassium carbonate / acetonitrile / Reflux
4: potassium carbonate / acetonitrile / Reflux
With
boron tribromide; potassium carbonate;
In
ethanol; dichloromethane; acetonitrile;
DOI:10.1016/j.bmcl.2012.10.022
- Guidance literature:
-
Multi-step reaction with 7 steps
1: potassium carbonate / N,N-dimethyl-formamide / Reflux
2: tetrahydrofuran / 65 °C
3: copper(ll) bromide / ethyl acetate / 70 °C
4: ethanol / Reflux
5: boron tribromide / dichloromethane / -78 °C
6: potassium carbonate / acetonitrile / Reflux
7: potassium carbonate / acetonitrile / Reflux
With
boron tribromide; potassium carbonate; copper(ll) bromide;
In
tetrahydrofuran; ethanol; dichloromethane; ethyl acetate; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/j.bmcl.2012.10.022
