C₃₈H₄₄FN₅O₅S

Base Information

Chemical Name:C₃₈H₄₄FN₅O₅S
CAS No.:1422251-99-7
Molecular Formula:C₃₈H₄₄FN₅O₅S
Molecular Weight:701.862
Hs Code.:

C<sub>38</sub>H<sub>44</sub>FN<sub>5</sub>O<sub>5</sub>S

Synonyms:

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Chemical Property of C₃₈H₄₄FN₅O₅S

Chemical Property:

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Technology Process of C₃₈H₄₄FN₅O₅S

There total 11 articles about C₃₈H₄₄FN₅O₅S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 154350-29-5
cyclopropanesulphonamide

: 1422252-12-7
C₃₅H₃₉FN₄O₄

: 1422251-99-7
C₃₈H₄₄FN₅O₅S

Guidance literature:: C₃₅H₃₉FN₄O₄; With 1,1'-carbonyldiimidazole; In tetrahydrofuran; at 50 ℃; for 2h; Inert atmosphere;

cyclopropanesulphonamide; With 1,8-diazabicyclo[5.4.0]undec-7-ene; In tetrahydrofuran; at 125 ℃; for 1h; Sealed tube;

With trifluoroacetic acid; In tetrahydrofuran;
DOI:10.1139/cjc-2012-0319

Reference yield:

: 1422252-10-5
C₂₉H₂₇FN₂O₅

: 1422251-99-7
C₃₈H₄₄FN₅O₅S

Guidance literature:: Multi-step reaction with 2 steps

1.1: O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; triethylamine / dimethyl sulfoxide / 20 °C / Inert atmosphere

1.2: 50 °C / pH 4 - 5

2.1: 1,1'-carbonyldiimidazole / tetrahydrofuran / 2 h / 50 °C / Inert atmosphere

2.2: 1 h / 125 °C / Sealed tube

With O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; triethylamine; 1,1'-carbonyldiimidazole; In tetrahydrofuran; dimethyl sulfoxide;
DOI:10.1139/cjc-2012-0319

Reference yield:

: C₂₂H₂₉NO₄

: 1422251-99-7
C₃₈H₄₄FN₅O₅S

Guidance literature:: Multi-step reaction with 5 steps

1.1: pyridinium tribromide / tetrahydrofuran; chloroform / 0 - 20 °C

2.1: tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; trifuran-2-yl-phosphane; potassium phosphate / water; 1,2-dimethoxyethane / Inert atmosphere; Reflux

3.1: hydrogenchloride / 1,4-dioxane / 3 h / 20 °C / Inert atmosphere

4.1: O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; triethylamine / dimethyl sulfoxide / 20 °C / Inert atmosphere

4.2: 50 °C / pH 4 - 5

5.1: 1,1'-carbonyldiimidazole / tetrahydrofuran / 2 h / 50 °C / Inert atmosphere

5.2: 1 h / 125 °C / Sealed tube

With hydrogenchloride; tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; potassium phosphate; pyridinium tribromide; trifuran-2-yl-phosphane; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; triethylamine; 1,1'-carbonyldiimidazole; In tetrahydrofuran; 1,4-dioxane; 1,2-dimethoxyethane; chloroform; water; dimethyl sulfoxide; 2.1: |Suzuki Coupling;
DOI:10.1139/cjc-2012-0319