chlorure de l'acide N-acetoxy chloro-2 (m.tolyl)-2 acetohydroximique

Base Information

• Chemical Name: chlorure de l'acide N-acetoxy chloro-2 (m.tolyl)-2 acetohydroximique
• CAS No.: 77484-39-0
• Molecular Formula: C₁₁H₁₁Cl₂NO₂
• Molecular Weight: 260.12
• Mol file: 77484-39-0.mol

Synonyms:

Chemical Property of chlorure de l'acide N-acetoxy chloro-2 (m.tolyl)-2 acetohydroximique

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of chlorure de l'acide N-acetoxy chloro-2 (m.tolyl)-2 acetohydroximique

There total 3 articles about chlorure de l'acide N-acetoxy chloro-2 (m.tolyl)-2 acetohydroximique which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

1-methyl-3-(2-nitrovinyl)benzene (22568-43-0,62248-93-5) + acetyl chloride (75-36-5) → chlorure de l'acide N-acetoxy chloro-2 (m.tolyl)-2 acetohydroximique (77484-39-0)

Guidance literature:

With titanium tetrachloride; In dichloromethane; at 0 ℃; for 5h; Product distribution; other Lewis acid;

Reference yield: 77.0%

1-methyl-3-(2-nitrovinyl)benzene (22568-43-0,62248-93-5) + acetyl chloride (75-36-5) → chloro-3 methyl-5 indolinone-2 (77484-19-6) + chlorure de l'acide N-acetoxy chloro-2 (m.tolyl)-2 acetohydroximique (77484-39-0)

Guidance literature:

With iron(III) chloride; In dichloromethane; at 0 ℃; for 5h; Product distribution; other Lewis acid;

Reference yield: 72.0%

1-methyl-3-(2-nitrovinyl)benzene (22568-43-0,62248-93-5) + acetyl chloride (75-36-5) → acide N-acetyl chloro-2 (m.tolyl)-2 acetohydroxamique (77484-29-8) + chlorure de l'acide N-acetoxy chloro-2 (m.tolyl)-2 acetohydroximique (77484-39-0)

Guidance literature:

With aluminium trichloride; In dichloromethane; at 0 ℃; for 5h; Product distribution; other Lewis acid;

upstream raw materials:

1-methyl-3-(2-nitrovinyl)benzene

acetyl chloride

Refernces