C₁₈H₁₇FNO₄P

Base Information

• Chemical Name: C₁₈H₁₇FNO₄P
• CAS No.: 100072-89-7
• Molecular Formula: C₁₈H₁₇FNO₄P
• Molecular Weight: 361.309
• Mol file: 100072-89-7.mol

Synonyms:

Chemical Property of C₁₈H₁₇FNO₄P

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₈H₁₇FNO₄P

There total 4 articles about C₁₈H₁₇FNO₄P which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

benzene (71-43-2,26181-88-4,54682-86-9,13967-78-7,174973-66-1) → C18H17FNO4P (100072-89-7,100163-82-4)

Guidance literature:

Multi-step reaction with 3 steps

1: 66 percent / PCl₃ / AlCl₃ / benzene

2: 65 percent / SeO₂ / acetic acid

3: CD₂Cl₂ / 0.08 h / -78 °C

With selenium(IV) oxide; phosphorus trichloride; aluminium trichloride; In dichloromethane-d2; acetic acid; benzene;

Reference yield:

p-Fluorophenylacetic acid (405-50-5) → C18H17FNO4P (100072-89-7,100163-82-4)

Guidance literature:

Multi-step reaction with 3 steps

1: 66 percent / PCl₃ / AlCl₃ / benzene

2: 65 percent / SeO₂ / acetic acid

3: CD₂Cl₂ / 0.08 h / -78 °C

With selenium(IV) oxide; phosphorus trichloride; aluminium trichloride; In dichloromethane-d2; acetic acid; benzene;

Reference yield:

2-(4-fluorophenyl)-1-phenylethanone (347-91-1) → C18H17FNO4P (100072-89-7,100163-82-4)

Guidance literature:

Multi-step reaction with 2 steps

1: 65 percent / SeO₂ / acetic acid

2: CD₂Cl₂ / 0.08 h / -78 °C

With selenium(IV) oxide; In dichloromethane-d2; acetic acid;

upstream raw materials:

(4-fluorophenyl)phenylethanedione

2,8-dioxa-5-aza-1-phosphabicyclo<3.3.0>octane

2-(4-fluorophenyl)-1-phenylethanone

benzene

Refernces