2,4-Dimethoxy-6-(6-methyl-5,6,7,8-tetrahydro-[1,3]dioxolo[4,5-g]isoquinolin-5-ylmethyl)-phenylamine

Base Information

Chemical Name:2,4-Dimethoxy-6-(6-methyl-5,6,7,8-tetrahydro-[1,3]dioxolo[4,5-g]isoquinolin-5-ylmethyl)-phenylamine
CAS No.:131653-15-1
Molecular Formula:C₂₀H₂₄N₂O₄
Molecular Weight:356.422
Hs Code.:

Synonyms:

Suppliers and Price of 2,4-Dimethoxy-6-(6-methyl-5,6,7,8-tetrahydro-[1,3]dioxolo[4,5-g]isoquinolin-5-ylmethyl)-phenylamine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 2,4-Dimethoxy-6-(6-methyl-5,6,7,8-tetrahydro-[1,3]dioxolo[4,5-g]isoquinolin-5-ylmethyl)-phenylamine

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2,4-Dimethoxy-6-(6-methyl-5,6,7,8-tetrahydro-[1,3]dioxolo[4,5-g]isoquinolin-5-ylmethyl)-phenylamine

There total 10 articles about 2,4-Dimethoxy-6-(6-methyl-5,6,7,8-tetrahydro-[1,3]dioxolo[4,5-g]isoquinolin-5-ylmethyl)-phenylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 131653-16-2
5-(3,5-Dimethoxy-2-nitro-benzyl)-6-methyl-5,6,7,8-tetrahydro-[1,3]dioxolo[4,5-g]isoquinoline

: 131653-15-1
2,4-Dimethoxy-6-(6-methyl-5,6,7,8-tetrahydro-[1,3]dioxolo[4,5-g]isoquinolin-5-ylmethyl)-phenylamine

Guidance literature:: With hydrogenchloride; poudre de zinc; water; acetic acid;

Reference yield:

: 2150-37-0
methyl 3,5-dimethoxybenzoate

: 131653-15-1
2,4-Dimethoxy-6-(6-methyl-5,6,7,8-tetrahydro-[1,3]dioxolo[4,5-g]isoquinolin-5-ylmethyl)-phenylamine

Guidance literature:: Multi-step reaction with 9 steps

1: acide nitrique fumant, anhydride acetique / -20 °C

2: 98.5 percent / aq. KOH / methanol / 0.5 h / Heating

3: SOCl₂, triethylamine / benzene / 3 h / Heating

4: triethylamine / diethyl ether

5: benzoate d'argent, triethylamine / diethyl ether; acetonitrile

6: Roblot F_., Hocquemiller R_., Cave A_., J_. Chem_. Research ⁽¹⁹⁸⁹⁾ (S) 344-345 (M) 2637-2651

7: 75 percent / CHCl₃ / Heating

8: 98 percent / NaBH₄ / methanol / 0.08 h

9: 98 percent / acide acetique, H₂O, 12 N HCl, poudre de zinc

With hydrogenchloride; potassium hydroxide; sodium tetrahydroborate; thionyl chloride; acide nitrique fumant; benzoate d'argent; poudre de zinc; water; acetic anhydride; acetic acid; triethylamine; In methanol; diethyl ether; chloroform; acetonitrile; benzene;

Reference yield:

: 109069-76-3
3,5-dimethoxy-2-nitrobenzoyl chloride

: 131653-15-1
2,4-Dimethoxy-6-(6-methyl-5,6,7,8-tetrahydro-[1,3]dioxolo[4,5-g]isoquinolin-5-ylmethyl)-phenylamine

Guidance literature:: Multi-step reaction with 6 steps

1: triethylamine / diethyl ether

2: benzoate d'argent, triethylamine / diethyl ether; acetonitrile

3: Roblot F_., Hocquemiller R_., Cave A_., J_. Chem_. Research ⁽¹⁹⁸⁹⁾ (S) 344-345 (M) 2637-2651

4: 75 percent / CHCl₃ / Heating

5: 98 percent / NaBH₄ / methanol / 0.08 h

6: 98 percent / acide acetique, H₂O, 12 N HCl, poudre de zinc

With hydrogenchloride; sodium tetrahydroborate; benzoate d'argent; poudre de zinc; water; acetic acid; triethylamine; In methanol; diethyl ether; chloroform; acetonitrile;