C₅₉H₇₁N₉O₁₇

Base Information Edit

Chemical Name:C₅₉H₇₁N₉O₁₇
CAS No.:1026452-09-4
Molecular Formula:C₅₉H₇₁N₉O₁₇
Molecular Weight:1178.26
Hs Code.:
Mol file:1026452-09-4.mol

C<sub>59</sub>H<sub>71</sub>N<sub>9</sub>O<sub>17</sub>

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Chemical Property of C₅₉H₇₁N₉O₁₇ Edit

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Technology Process of C₅₉H₇₁N₉O₁₇

There total 22 articles about C₅₉H₇₁N₉O₁₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 6515-21-5
4-methoxymethoxy-benzaldehyde

: 1026452-09-4
C₅₉H₇₁N₉O₁₇

Guidance literature:: Multi-step reaction with 21 steps

1: KOH / ethanol / 19 h / Ambient temperature

2: 1 N aq. NaOH / 0.33 h / 90 °C

3: 85 percent / BSA / CH₂Cl₂ / 5 h / 0 - 20 °C

4: 32.1 percent / diethyl ether; ethyl acetate / 0.17 h

5: 93.6 percent / Et₃N, DMAP / CH₂Cl₂ / 16 h / Ambient temperature

6: 72.1 percent / thiophenol, TFA / CH₂Cl₂ / 0.5 h / 0 °C

7: 49.1 percent / 2-ethoxy-N-ethoxycarbonyl-1,2-dihydroquinoline / CH₂Cl₂ / 14 h / Ambient temperature

8: DBU / toluene / 2.5 h / Ambient temperature

9: 98 percent / imidazole / dimethylformamide / 16 h / Ambient temperature

10: 87.3 percent / NaOH / methanol / 48 h / 30 °C

11: 32.6 percent / Et₃N, EEDQ / CH₂Cl₂ / 33 h / Ambient temperature

12: 21.2 percent / acetone; toluene / 1.5 h / 0 °C / Irradiation

13: 99.9 percent / 67percent AcOH / 28 h / 25 °C

14: 86.5 percent / EDC*HCl, DMAP / CH₂Cl₂ / 12 h / Ambient temperature

15: 4 N HCl, anisole / dioxane / 0.5 h / Ambient temperature

16: Et₃N, HOBT, EDC*HCl / CH₂Cl₂ / 1 h / Ambient temperature

17: 4 N HCl, anisole / dioxane / 0.5 h / Ambient temperature

18: Et₃N, HOBT, EDC*HCl / CH₂Cl₂ / 8 h / Ambient temperature

19: 82.6 percent / Zn, 90percent AcOH / Ambient temperature

20: EDC*HCl / CH₂Cl₂; dimethylformamide / Ambient temperature

21: TFA, anisole / 0.5 h / Ambient temperature

With 1H-imidazole; hydrogenchloride; benzenesulfonamide; dmap; potassium hydroxide; sodium hydroxide; benzotriazol-1-ol; acetic acid; thiophenol; methoxybenzene; 1,8-diazabicyclo[5.4.0]undec-7-ene; N-ethoxycarbonyl-2-ethoxy-1,2-dihydroquinoline; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; trifluoroacetic acid; zinc; In 1,4-dioxane; methanol; diethyl ether; ethanol; dichloromethane; ethyl acetate; N,N-dimethyl-formamide; acetone; toluene;
DOI:10.1248/cpb.45.236

Reference yield:

: 123-08-0,65581-83-1
4-hydroxy-benzaldehyde

: 1026452-09-4
C₅₉H₇₁N₉O₁₇

Guidance literature:: Multi-step reaction with 22 steps

1: 88.7 percent / Et₃N / tetrahydrofuran / 1 h / Ambient temperature

2: KOH / ethanol / 19 h / Ambient temperature

3: 1 N aq. NaOH / 0.33 h / 90 °C

4: 85 percent / BSA / CH₂Cl₂ / 5 h / 0 - 20 °C

5: 32.1 percent / diethyl ether; ethyl acetate / 0.17 h

6: 93.6 percent / Et₃N, DMAP / CH₂Cl₂ / 16 h / Ambient temperature

7: 72.1 percent / thiophenol, TFA / CH₂Cl₂ / 0.5 h / 0 °C

8: 49.1 percent / 2-ethoxy-N-ethoxycarbonyl-1,2-dihydroquinoline / CH₂Cl₂ / 14 h / Ambient temperature

9: DBU / toluene / 2.5 h / Ambient temperature

10: 98 percent / imidazole / dimethylformamide / 16 h / Ambient temperature

11: 87.3 percent / NaOH / methanol / 48 h / 30 °C

12: 32.6 percent / Et₃N, EEDQ / CH₂Cl₂ / 33 h / Ambient temperature

13: 21.2 percent / acetone; toluene / 1.5 h / 0 °C / Irradiation

14: 99.9 percent / 67percent AcOH / 28 h / 25 °C

15: 86.5 percent / EDC*HCl, DMAP / CH₂Cl₂ / 12 h / Ambient temperature

16: 4 N HCl, anisole / dioxane / 0.5 h / Ambient temperature

17: Et₃N, HOBT, EDC*HCl / CH₂Cl₂ / 1 h / Ambient temperature

18: 4 N HCl, anisole / dioxane / 0.5 h / Ambient temperature

19: Et₃N, HOBT, EDC*HCl / CH₂Cl₂ / 8 h / Ambient temperature

20: 82.6 percent / Zn, 90percent AcOH / Ambient temperature

21: EDC*HCl / CH₂Cl₂; dimethylformamide / Ambient temperature

22: TFA, anisole / 0.5 h / Ambient temperature

With 1H-imidazole; hydrogenchloride; benzenesulfonamide; dmap; potassium hydroxide; sodium hydroxide; benzotriazol-1-ol; acetic acid; thiophenol; methoxybenzene; 1,8-diazabicyclo[5.4.0]undec-7-ene; N-ethoxycarbonyl-2-ethoxy-1,2-dihydroquinoline; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; trifluoroacetic acid; zinc; In tetrahydrofuran; 1,4-dioxane; methanol; diethyl ether; ethanol; dichloromethane; ethyl acetate; N,N-dimethyl-formamide; acetone; toluene;
DOI:10.1248/cpb.45.236

Reference yield:

: 125774-95-0
O-methoxymethyl-β-hydroxytyrosine

: 1026452-09-4
C₅₉H₇₁N₉O₁₇

Guidance literature:: Multi-step reaction with 20 steps

1: 1 N aq. NaOH / 0.33 h / 90 °C

2: 85 percent / BSA / CH₂Cl₂ / 5 h / 0 - 20 °C

3: 32.1 percent / diethyl ether; ethyl acetate / 0.17 h

4: 93.6 percent / Et₃N, DMAP / CH₂Cl₂ / 16 h / Ambient temperature

5: 72.1 percent / thiophenol, TFA / CH₂Cl₂ / 0.5 h / 0 °C

6: 49.1 percent / 2-ethoxy-N-ethoxycarbonyl-1,2-dihydroquinoline / CH₂Cl₂ / 14 h / Ambient temperature

7: DBU / toluene / 2.5 h / Ambient temperature

8: 98 percent / imidazole / dimethylformamide / 16 h / Ambient temperature

9: 87.3 percent / NaOH / methanol / 48 h / 30 °C

10: 32.6 percent / Et₃N, EEDQ / CH₂Cl₂ / 33 h / Ambient temperature

11: 21.2 percent / acetone; toluene / 1.5 h / 0 °C / Irradiation

12: 99.9 percent / 67percent AcOH / 28 h / 25 °C

13: 86.5 percent / EDC*HCl, DMAP / CH₂Cl₂ / 12 h / Ambient temperature

14: 4 N HCl, anisole / dioxane / 0.5 h / Ambient temperature

15: Et₃N, HOBT, EDC*HCl / CH₂Cl₂ / 1 h / Ambient temperature

16: 4 N HCl, anisole / dioxane / 0.5 h / Ambient temperature

17: Et₃N, HOBT, EDC*HCl / CH₂Cl₂ / 8 h / Ambient temperature

18: 82.6 percent / Zn, 90percent AcOH / Ambient temperature

19: EDC*HCl / CH₂Cl₂; dimethylformamide / Ambient temperature

20: TFA, anisole / 0.5 h / Ambient temperature

With 1H-imidazole; hydrogenchloride; benzenesulfonamide; dmap; sodium hydroxide; benzotriazol-1-ol; acetic acid; thiophenol; methoxybenzene; 1,8-diazabicyclo[5.4.0]undec-7-ene; N-ethoxycarbonyl-2-ethoxy-1,2-dihydroquinoline; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; trifluoroacetic acid; zinc; In 1,4-dioxane; methanol; diethyl ether; dichloromethane; ethyl acetate; N,N-dimethyl-formamide; acetone; toluene;
DOI:10.1248/cpb.45.236