Propanoyl chloride, 3-[[(1,1-dimethylethyl)diphenylsilyl]oxy]-

Base Information

Chemical Name:Propanoyl chloride, 3-[[(1,1-dimethylethyl)diphenylsilyl]oxy]-
CAS No.:105198-75-2
Molecular Formula:C19H23ClO2Si
Molecular Weight:346.929
Hs Code.:
Mol file:105198-75-2.mol

Synonyms:

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Chemical Property of Propanoyl chloride, 3-[[(1,1-dimethylethyl)diphenylsilyl]oxy]-

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

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Technology Process of Propanoyl chloride, 3-[[(1,1-dimethylethyl)diphenylsilyl]oxy]-

There total 4 articles about Propanoyl chloride, 3-[[(1,1-dimethylethyl)diphenylsilyl]oxy]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 310409-17-7
methyl 3-(tert-butyldiphenylsilyloxy)propanoic acid

: 105198-75-2
3-(tert-butyldiphenylsilyloxy)propanoyl chloride

Guidance literature:: With oxalyl dichloride; In dichloromethane; at 20 ℃; for 15h;
DOI:10.1016/j.tet.2006.09.096

Reference yield:

: 166194-08-7
methyl 3-<(tert-butyldiphenylsilyl)oxy>propionate

: 105198-75-2
3-(tert-butyldiphenylsilyloxy)propanoyl chloride

Guidance literature:: Multi-step reaction with 2 steps

1: 68 percent / lithium hydroxide / H₂O; methanol / 5 h / 20 °C

2: oxalyl chloride / benzene; dimethylformamide / 1.5 h / 20 °C

With lithium hydroxide; oxalyl dichloride; In methanol; water; N,N-dimethyl-formamide; benzene;
DOI:10.1016/j.bmc.2006.03.051

Reference yield:

: 58479-61-1
tert-butylchlorodiphenylsilane

: 105198-75-2
3-(tert-butyldiphenylsilyloxy)propanoyl chloride

Guidance literature:: Multi-step reaction with 3 steps

1: 96 percent / imidazole / CH₂Cl₂ / 14 h / 20 °C

2: 99 percent / sodium hydroxide / ethanol; H₂O / 6 h / 20 °C

3: 100 percent / oxalyl chloride / CH₂Cl₂ / 15 h / 20 °C

With 1H-imidazole; sodium hydroxide; oxalyl dichloride; In ethanol; dichloromethane; water;
DOI:10.1016/j.tet.2006.09.096