3,6,9,17,25-pentatosyl-3,6,9,17,25,31,32,33-octaazatetracyclo<25.3.1.1^11,15.1^19,23>tritriaconta-1(31),11(32),12,14,19(33),20,22,27,29-nonaene

Base Information

• Chemical Name: 3,6,9,17,25-pentatosyl-3,6,9,17,25,31,32,33-octaazatetracyclo<25.3.1.1^11,15.1^19,23>tritriaconta-1(31),11(32),12,14,19(33),20,22,27,29-nonaene
• CAS No.: 125683-04-7
• Molecular Formula: C₆₀H₆₄N₈O₁₀S₅
• Molecular Weight: 1217.55

Synonyms:

Chemical Property of 3,6,9,17,25-pentatosyl-3,6,9,17,25,31,32,33-octaazatetracyclo<25.3.1.1^11,15.1^19,23>tritriaconta-1(31),11(32),12,14,19(33),20,22,27,29-nonaene

Chemical Property:

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Safty Information:

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MSDS Files:

Useful:

Technology Process of 3,6,9,17,25-pentatosyl-3,6,9,17,25,31,32,33-octaazatetracyclo<25.3.1.1^11,15.1^19,23>tritriaconta-1(31),11(32),12,14,19(33),20,22,27,29-nonaene

There total 7 articles about 3,6,9,17,25-pentatosyl-3,6,9,17,25,31,32,33-octaazatetracyclo<25.3.1.1^11,15.1^19,23>tritriaconta-1(31),11(32),12,14,19(33),20,22,27,29-nonaene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 35.0%

N,N’,N”-tris(p-toluenesulfonyl)diethylenetriamine N,N-disodium salt (52601-80-6) + 2,6-bis<pyridin-2-yl>methyl>-N-tosylamino>methyl>pyridine (125683-03-6) → 3,6,9,17,25-pentatosyl-3,6,9,17,25,31,32,33-octaazatetracyclo<25.3.1.111,15.119,23>tritriaconta-1(31),11(32),12,14,19(33),20,22,27,29-nonaene (125683-04-7)

Guidance literature:

In N,N-dimethyl-formamide; at 90 ℃; for 3h;

DOI:10.1002/hlca.19890720525

Reference yield:

2,6-bis(aminomethyl)pyridine (34984-16-2) → 3,6,9,17,25-pentatosyl-3,6,9,17,25,31,32,33-octaazatetracyclo<25.3.1.111,15.119,23>tritriaconta-1(31),11(32),12,14,19(33),20,22,27,29-nonaene (125683-04-7)

Guidance literature:

Multi-step reaction with 5 steps

1: 94 percent

2: Na / methanol / 2 h / Heating

3: 51 percent / dimethylformamide / 5 h / 90 °C

4: 98 percent / Et₃N / CH₂Cl₂ / 3 h / Ambient temperature

5: 35 percent / dimethylformamide / 3 h / 90 °C

With sodium; triethylamine; In methanol; dichloromethane; N,N-dimethyl-formamide;

DOI:10.1002/hlca.19890720525

Reference yield:

1,4,7-tritosyl-1,4,7-triazaheptane (56187-04-3) → 3,6,9,17,25-pentatosyl-3,6,9,17,25,31,32,33-octaazatetracyclo<25.3.1.111,15.119,23>tritriaconta-1(31),11(32),12,14,19(33),20,22,27,29-nonaene (125683-04-7)

Guidance literature:

Multi-step reaction with 2 steps

1: Na / 2 h / Heating

2: 35 percent / dimethylformamide / 3 h / 90 °C

With sodium; In N,N-dimethyl-formamide;

DOI:10.1002/hlca.19890720525

upstream raw materials:

N,N’,N”-tris(p-toluenesulfonyl)diethylenetriamine N,N-disodium salt

2,6-bis<pyridin-2-yl>methyl>-N-tosylamino>methyl>pyridine

2,6-bis(aminomethyl)pyridine

1,4,7-tritosyl-1,4,7-triazaheptane

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