2H-1,2-Oxazine, 2-(4-chlorophenyl)-3,6-dihydro-4,5-dimethyl-

Base Information

Chemical Name:2H-1,2-Oxazine, 2-(4-chlorophenyl)-3,6-dihydro-4,5-dimethyl-
CAS No.:105207-76-9
Molecular Formula:C12H14ClNO
Molecular Weight:223.702
Hs Code.:
DSSTox Substance ID:DTXSID10460914
Nikkaji Number:J767.677H
Wikidata:Q82285092

Synonyms:105207-76-9;2H-1,2-Oxazine, 2-(4-chlorophenyl)-3,6-dihydro-4,5-dimethyl-;DTXSID10460914

Suppliers and Price of 2H-1,2-Oxazine, 2-(4-chlorophenyl)-3,6-dihydro-4,5-dimethyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2H-1,2-Oxazine, 2-(4-chlorophenyl)-3,6-dihydro-4,5-dimethyl-

Chemical Property:

XLogP3:2.8
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:1
Exact Mass:223.0763918
Heavy Atom Count:15
Complexity:256

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=C(CON(C1)C2=CC=C(C=C2)Cl)C

Technology Process of 2H-1,2-Oxazine, 2-(4-chlorophenyl)-3,6-dihydro-4,5-dimethyl-

There total 4 articles about 2H-1,2-Oxazine, 2-(4-chlorophenyl)-3,6-dihydro-4,5-dimethyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 100-00-5
4-chlorobenzonitrile

: 513-81-5
2,3-dimethyl-buta-1,3-diene

: 105207-76-9
2-(4-chlorophenyl)-4,5-dimethyl-3,6-dihydro-2H-[1,2]-oxazine

Guidance literature:: With dichloro bis(acetonitrile) palladium(II); 1,10-Phenanthroline; phenyl formate; triethylamine; In acetonitrile; at 140 ℃; for 4h; Inert atmosphere; Sealed tube; Schlenk technique;
DOI:10.1002/cctc.201801223

Reference yield:

: 100-00-5
4-chlorobenzonitrile

: 513-81-5
2,3-dimethyl-buta-1,3-diene

: 105207-76-9
2-(4-chlorophenyl)-4,5-dimethyl-3,6-dihydro-2H-[1,2]-oxazine

: 106-47-8
4-chloro-aniline

Guidance literature:: With carbon monoxide; {Pd([1,10]phenanthroline)2}[BF₄]2; triethylamine; In tetrahydrofuran; at 100 ℃; for 6h; under 7500.75 Torr; Title compound not separated from byproducts.;
DOI:10.1021/jo0260589