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Technology Process of NC(CH3)CHN2CS(CH3)N2C(CH3)CHN2CS(CH3)NNi

NC(CH3)CHN2CS(CH3)N2C(CH3)CHN2CS(CH3)NNi

Base Information
  • Chemical Name:NC(CH3)CHN2CS(CH3)N2C(CH3)CHN2CS(CH3)NNi
  • CAS No.:105154-39-0
  • Molecular Formula:C10H14N8NiS2
  • Molecular Weight:369.097
  • Hs Code.:
NC(CH<sub>3</sub>)CHN<sub>2</sub>CS(CH<sub>3</sub>)N<sub>2</sub>C(CH<sub>3</sub>)CHN<sub>2</sub>CS(CH<sub>3</sub>)NNi

Synonyms:

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Chemical Property of NC(CH3)CHN2CS(CH3)N2C(CH3)CHN2CS(CH3)NNi
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Technology Process of NC(CH3)CHN2CS(CH3)N2C(CH3)CHN2CS(CH3)NNi

There total 2 articles about NC(CH3)CHN2CS(CH3)N2C(CH3)CHN2CS(CH3)NNi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 16.0%

nickel(II) chloride hexahydrate

nickel(II) chloride hexahydrate

1H(+)-S-methylisothiocarbonohydrazidium iodide
37839-01-3,67708-03-6

1H(+)-S-methylisothiocarbonohydrazidium iodide

2-oxopropanal
78-98-8

2-oxopropanal

NCHC(CH<sub>3</sub>)N<sub>2</sub>CS(CH<sub>3</sub>)N<sub>2</sub>CHC(CH<sub>3</sub>)N<sub>2</sub>CS(CH<sub>3</sub>)NNi
105154-39-0,105154-40-3

NCHC(CH3)N2CS(CH3)N2CHC(CH3)N2CS(CH3)NNi

NC(CH<sub>3</sub>)CHN<sub>2</sub>CS(CH<sub>3</sub>)N<sub>2</sub>C(CH<sub>3</sub>)CHN<sub>2</sub>CS(CH<sub>3</sub>)NNi
105154-39-0,105154-40-3

NC(CH3)CHN2CS(CH3)N2C(CH3)CHN2CS(CH3)NNi

NC(CH<sub>3</sub>)CHN<sub>2</sub>CS(CH<sub>3</sub>)N<sub>2</sub>CHC(CH<sub>3</sub>)N<sub>2</sub>CS(CH<sub>3</sub>)NNi
106256-53-5

NC(CH3)CHN2CS(CH3)N2CHC(CH3)N2CS(CH3)NNi

Guidance literature:
With pyridine; In ethanol; water; pyridine and methylglyoxal aq. soln. added to soln. of NiCl2*6H2O and S-methylisothiocarbohydrazide hydroiodide in 85% aq. ethanol; mixt. heated to 70°C for 3 h; cooled; ppt. filtered off; washed (acetone); chromy. (silica gel, chloroform); elem. anal.;

Reference yield: 16.0%

nickel(II) chloride hexahydrate

nickel(II) chloride hexahydrate

1H(+)-S-methylisothiocarbonohydrazidium iodide
37839-01-3,67708-03-6

1H(+)-S-methylisothiocarbonohydrazidium iodide

2-oxopropanal
78-98-8

2-oxopropanal

NCHC(CH<sub>3</sub>)N<sub>2</sub>CS(CH<sub>3</sub>)N<sub>2</sub>CHC(CH<sub>3</sub>)N<sub>2</sub>CS(CH<sub>3</sub>)NNi
105154-39-0,105154-40-3

NCHC(CH3)N2CS(CH3)N2CHC(CH3)N2CS(CH3)NNi

NC(CH<sub>3</sub>)CHN<sub>2</sub>CS(CH<sub>3</sub>)N<sub>2</sub>C(CH<sub>3</sub>)CHN<sub>2</sub>CS(CH<sub>3</sub>)NNi
105154-39-0,105154-40-3

NC(CH3)CHN2CS(CH3)N2C(CH3)CHN2CS(CH3)NNi

NC(CH<sub>3</sub>)CHN<sub>2</sub>CS(CH<sub>3</sub>)N<sub>2</sub>CHC(CH<sub>3</sub>)N<sub>2</sub>CS(CH<sub>3</sub>)NNi
106256-53-5

NC(CH3)CHN2CS(CH3)N2CHC(CH3)N2CS(CH3)NNi

Guidance literature:
With pyridine; In ethanol; water; pyridine and methylglyoxal aq. soln. added to soln. of NiCl2*6H2O and S-methylisothiocarbohydrazide hydroiodide in 85% aq. ethanol; mixt. heated to 70°C for 3 h; cooled; ppt. filtered off; washed (acetone); chromy. (silica gel, chloroform); elem. anal.;
upstream raw materials:

1H(+)-S-methylisothiocarbonohydrazidium iodide

2-oxopropanal

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