1-benzyloxy-14,14,15,15,16,16,16-heptafluorohexadecane

Base Information

• Chemical Name: 1-benzyloxy-14,14,15,15,16,16,16-heptafluorohexadecane
• CAS No.: 108330-72-9
• Molecular Formula: C₂₃H₃₃F₇O
• Molecular Weight: 458.503

Synonyms:

Chemical Property of 1-benzyloxy-14,14,15,15,16,16,16-heptafluorohexadecane

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of 1-benzyloxy-14,14,15,15,16,16,16-heptafluorohexadecane

There total 4 articles about 1-benzyloxy-14,14,15,15,16,16,16-heptafluorohexadecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

9-decen-1-yl acetate (50816-18-7) → 1-benzyloxy-14,14,15,15,16,16,16-heptafluorohexadecane (108330-72-9)

Guidance literature:

Multi-step reaction with 5 steps

1: Fe₃(CO)12 / 5.5 h / 80 °C

2: Zn powder / acetic acid; diethyl ether / 1 h / Ambient temperature

3: 5 percent methanolic KOH / 2 h / Ambient temperature

4: 85 percent / triphenylphosphine dibromide / dimethylformamide; acetonitrile

5: 40 percent / 0.1 M Li₂CuCl₄ / tetrahydrofuran / 5 h / Ambient temperature

With potassium hydroxide; zinc; dibromotriphenylphosphorane; dilithium tetrachlorocuprate; triiron dodecarbonyl; In tetrahydrofuran; diethyl ether; acetic acid; N,N-dimethyl-formamide; acetonitrile;

DOI:10.1248/cpb.35.647

Reference yield:

11,11,12,12,13,13,13-heptafluorotridecan-1-ol (102197-75-1) → 1-benzyloxy-14,14,15,15,16,16,16-heptafluorohexadecane (108330-72-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 85 percent / triphenylphosphine dibromide / dimethylformamide; acetonitrile

2: 40 percent / 0.1 M Li₂CuCl₄ / tetrahydrofuran / 5 h / Ambient temperature

With dibromotriphenylphosphorane; dilithium tetrachlorocuprate; In tetrahydrofuran; N,N-dimethyl-formamide; acetonitrile;

DOI:10.1248/cpb.35.647

Reference yield:

11,11,12,12,13,13,13-heptafluorotridecanyl acetate (102197-74-0) → 1-benzyloxy-14,14,15,15,16,16,16-heptafluorohexadecane (108330-72-9)

Guidance literature:

Multi-step reaction with 3 steps

1: 5 percent methanolic KOH / 2 h / Ambient temperature

2: 85 percent / triphenylphosphine dibromide / dimethylformamide; acetonitrile

3: 40 percent / 0.1 M Li₂CuCl₄ / tetrahydrofuran / 5 h / Ambient temperature

With potassium hydroxide; dibromotriphenylphosphorane; dilithium tetrachlorocuprate; In tetrahydrofuran; N,N-dimethyl-formamide; acetonitrile;

DOI:10.1248/cpb.35.647

upstream raw materials:

9-decen-1-yl acetate

11,11,12,12,13,13,13-heptafluorotridecan-1-ol

11,11,12,12,13,13,13-heptafluorotridecanyl acetate

Acetic acid 11,11,12,12,13,13,13-heptafluoro-9-iodo-tridecyl ester

Downstream raw materials:

C₃₁H₅₁F₇NO₆P

(R)-4-[(R)-1-Benzyloxy-2-(14,14,15,15,16,16,16-heptafluoro-hexadecyloxy)-ethyl]-2,2-dimethyl-[1,3]dioxolane

(2R,3R)-3-Benzyloxy-4-(14,14,15,15,16,16,16-heptafluoro-hexadecyloxy)-butane-1,2-diol

(R)-2-Benzyloxy-3-(14,14,15,15,16,16,16-heptafluoro-hexadecyloxy)-propionaldehyde

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