C₄₄H₇₀O₇SSi

Base Information

Chemical Name:C₄₄H₇₀O₇SSi
CAS No.:128322-43-0
Molecular Formula:C₄₄H₇₀O₇SSi
Molecular Weight:771.187
Hs Code.:

C<sub>44</sub>H<sub>70</sub>O<sub>7</sub>SSi

Synonyms:

Suppliers and Price of C₄₄H₇₀O₇SSi

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₄₄H₇₀O₇SSi

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₄₄H₇₀O₇SSi

There total 11 articles about C₄₄H₇₀O₇SSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 75-77-4
chloro-trimethyl-silane

: 128292-46-6
C₄₁H₆₂O₇S

: 128322-43-0
C₄₄H₇₀O₇SSi

Guidance literature:: With pyridine;

Reference yield:

: 7154-75-8
4-methylpentyne

: 128322-43-0
C₄₄H₇₀O₇SSi

Guidance literature:: Multi-step reaction with 9 steps

1: 96 percent / (PhMe₂Si)2CuLi*LiCN / tetrahydrofuran / 0.5 h / 0 °C

3: ICl / CH₂Cl₂ / 2 h / Heating

4: 98 percent / Et₃N / CHCl₃ / 3 h / 0 deg C -> RT

5: (n-Bu)3SnH, AIBN / benzene / 12 h / Heating

6: 65 percent / KOH, DMSO / 16 h / 60 °C

7: 75 percent / KHCO₃, 70percent aq. H₂O₂ / tetrahydrofuran; methanol / Heating

8: 88 percent / pyridine, DMAP / CH₂Cl₂ / 72 h / 0 °C

9: 90 percent / pyridine

With pyridine; dmap; potassium hydroxide; 2,2'-azobis(isobutyronitrile); dihydrogen peroxide; tri-n-butyl-tin hydride; Iodine monochloride; potassium hydrogencarbonate; (PhMe₂Si)2CuLi*LiCN; dimethyl sulfoxide; triethylamine; In tetrahydrofuran; methanol; dichloromethane; chloroform; benzene;

Reference yield:

: (1-Bromo-4-methyl-pentyl)-chloro-dimethyl-silane

: 128322-43-0
C₄₄H₇₀O₇SSi

Guidance literature:: Multi-step reaction with 6 steps

1: 98 percent / Et₃N / CHCl₃ / 3 h / 0 deg C -> RT

2: (n-Bu)3SnH, AIBN / benzene / 12 h / Heating

3: 65 percent / KOH, DMSO / 16 h / 60 °C

4: 75 percent / KHCO₃, 70percent aq. H₂O₂ / tetrahydrofuran; methanol / Heating

5: 88 percent / pyridine, DMAP / CH₂Cl₂ / 72 h / 0 °C

6: 90 percent / pyridine

With pyridine; dmap; potassium hydroxide; 2,2'-azobis(isobutyronitrile); dihydrogen peroxide; tri-n-butyl-tin hydride; potassium hydrogencarbonate; dimethyl sulfoxide; triethylamine; In tetrahydrofuran; methanol; dichloromethane; chloroform; benzene;