4-(4-Fluoro-benzenesulfonyl)-piperidine hydrochloride

Base Information

• Chemical Name: 4-(4-Fluoro-benzenesulfonyl)-piperidine hydrochloride
• CAS No.: 105283-71-4
• Molecular Formula: C11H14FNO2S.ClH
• Molecular Weight: 279.75900
• Hs Code.: 2933399990
• Mol file: 105283-71-4.mol

Synonyms:Piperidine, 4-[(4-fluorophenyl)sulfonyl]-, hydrochloride (1:1);Piperidine, 4-[(4-fluorophenyl)sulfonyl]-, hydrochloride (9CI);

Chemical Property of 4-(4-Fluoro-benzenesulfonyl)-piperidine hydrochloride

Chemical Property:

• PSA: 54.55000
• LogP: 3.56300

Purity/Quality:

97% ^*data from raw suppliers

4-((4-Fluorophenyl)sulfonyl)piperidineHydrochloride ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 4-(4-Fluoro-benzenesulfonyl)-piperidine hydrochloride

There total 9 articles about 4-(4-Fluoro-benzenesulfonyl)-piperidine hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

tert-butyl 4-[(4-fluorophenyl)sulfonyl]piperidine-1-carboxylate (226398-50-1) → 4-[(4-fluorophenyl)sulfonyl]piperidine hydrochloride (105283-71-4)

Guidance literature:

With hydrogenchloride; ethyl acetate; In methanol; at 20 ℃;

DOI:10.1021/jm051034q

Reference yield: 94.0%

tert-butyl 4-[(4-fluorophenyl)sulfonyl]piperidine-1-carboxylate (226398-50-1) → 4-((4-fluorophenyl)sulfonyl)piperidine hydrochloride salt (105283-71-4)

Guidance literature:

With hydrogenchloride; In 1,4-dioxane; at 20 ℃; for 4h;

Reference yield:

4N-hydrogen chloride + tert-butyl 4-[(4-fluorophenyl)sulfonyl]piperidine-1-carboxylate (226398-50-1) → 4-[(4-fluorophenyl)sulfonyl]piperidine hydrochloride (105283-71-4)

Guidance literature:

In methanol; ethyl acetate;

upstream raw materials:

tert-butyl 4-[(4-fluorophenyl)sulfonyl]piperidine-1-carboxylate

t-butyl 4-hydroxy piperidine-1-carboxylate

1-(tert-butoxycarbonyl)piperidin-4-yl methanesulfonate

tert-butyl 4-[(4-fluorophenyl)sulfanyl]piperidine-1-carboxylate

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