pyridine-2-carbaldehyde-N-methylnitrone

Base Information

• Chemical Name: pyridine-2-carbaldehyde-N-methylnitrone
• CAS No.: 925933-59-1
• Molecular Formula: C₇H₈N₂O
• Molecular Weight: 136.153
• Mol file: 925933-59-1.mol

Synonyms:

Chemical Property of pyridine-2-carbaldehyde-N-methylnitrone

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of pyridine-2-carbaldehyde-N-methylnitrone

There total 1 articles about pyridine-2-carbaldehyde-N-methylnitrone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

pyridine-2-carbaldehyde (1121-60-4) + N-methylhydroxyamine hydrochloride (4229-44-1) → pyridine-2-carbaldehyde-N-methylnitrone (20251-40-5,925933-59-1,182487-40-7)

Guidance literature:

With triethylamine; In chloroform; for 22h;

DOI:10.1248/cpb.50.908

Reference yield: 67.0%

mercury dibromide + pyridine-2-carbaldehyde-N-methylnitrone (20251-40-5,925933-59-1,182487-40-7) → (HgBr2)2(2-pyridyl-N-methylnitrone)

Guidance literature:

In methanol; at 46.84 - 56.84 ℃; for 0.333333h;

DOI:10.1039/c7dt00050b

Reference yield: 67.0%

mercury(II) iodide + pyridine-2-carbaldehyde-N-methylnitrone (20251-40-5,925933-59-1,182487-40-7) → (HgI2)2(2-pyridyl-N-methylnitrone)

Guidance literature:

In methanol; at 46.84 - 56.84 ℃; for 0.333333h;

DOI:10.1039/c7dt00050b

upstream raw materials:

pyridine-2-carbaldehyde

N-methylhydroxyamine hydrochloride