methyl uronate

Base Information

• Chemical Name: methyl uronate
• CAS No.: 146352-70-7
• Molecular Formula: C₂₃H₂₇NO₇
• Molecular Weight: 429.47

Synonyms:

Chemical Property of methyl uronate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of methyl uronate

There total 2 articles about methyl uronate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

methanol (67-56-1) + 2-(N-benzyl,N-benzyloxycarbonyl)amino-2,3-dideoxy-β-D-arabino-furanurono-6,1-lactone (146352-67-2) → methyl uronate (146352-70-7,146352-71-8)

Guidance literature:

With methanesulfonic acid; at 20 ℃; Yield given;

DOI:10.1016/S0040-4020(01)88357-5

Reference yield:

methanol (67-56-1) + (+/-)-2-(N-benzyl,N-benzyloxycarbonyl)amino-2,3-dideoxy-β-DL-arabino-furanurono-6,1-lactone (146352-66-1,146352-67-2) → methyl uronate (146352-70-7,146352-71-8)

Guidance literature:

With methanesulfonic acid; at 20 ℃;

DOI:10.1016/S0040-4020(01)88357-5

Reference yield: 72.0%

methyl uronate (146352-70-7,146352-71-8) → methyl 2-(N-benzyl,N-benzyloxycarbonyl)amino-2,3-dideoxy-αβ-D-arabino-hexofuranoside (146352-72-9,146352-73-0)

Guidance literature:

With lithium borohydride; In tetrahydrofuran; at 20 ℃;

DOI:10.1016/S0040-4020(01)88357-5

upstream raw materials:

methanol

2-(N-benzyl,N-benzyloxycarbonyl)amino-2,3-dideoxy-β-D-arabino-furanurono-6,1-lactone

(+/-)-2-(N-benzyl,N-benzyloxycarbonyl)amino-2,3-dideoxy-β-DL-arabino-furanurono-6,1-lactone

Downstream raw materials:

methyl 2-(N-benzyl,N-benzyloxycarbonyl)amino-2,3-dideoxy-αβ-D-arabino-hexofuranoside

methyl 2-(N-benzyl,N-benzyloxycarbonyl)amino-2,3-dideoxy-αβ-DL-arabino-hexofuranoside

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