(+/-)-7-Dimethylamino-4-thiobenzamido-3,10,12-trihydroxy-1,4β,4aα,5,5aα,6,11,12aα-oktahydro-1,11-dioxo-6-thianaphthacen-2-carboxamid, racemat

Base Information

Chemical Name:(+/-)-7-Dimethylamino-4-thiobenzamido-3,10,12-trihydroxy-1,4β,4aα,5,5aα,6,11,12aα-oktahydro-1,11-dioxo-6-thianaphthacen-2-carboxamid, racemat
CAS No.:70098-67-8
Molecular Formula:C₂₇H₂₅N₃O₆S₂
Molecular Weight:551.644
Hs Code.:

(+/-)-7-Dimethylamino-4-thiobenzamido-3,10,12-trihydroxy-1,4β,4aα,5,5aα,6,11,12aα-oktahydro-1,11-dioxo-6-thianaphthacen-2-carboxamid, racemat

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Chemical Property of (+/-)-7-Dimethylamino-4-thiobenzamido-3,10,12-trihydroxy-1,4β,4aα,5,5aα,6,11,12aα-oktahydro-1,11-dioxo-6-thianaphthacen-2-carboxamid, racemat

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Technology Process of (+/-)-7-Dimethylamino-4-thiobenzamido-3,10,12-trihydroxy-1,4β,4aα,5,5aα,6,11,12aα-oktahydro-1,11-dioxo-6-thianaphthacen-2-carboxamid, racemat

There total 2 articles about (+/-)-7-Dimethylamino-4-thiobenzamido-3,10,12-trihydroxy-1,4β,4aα,5,5aα,6,11,12aα-oktahydro-1,11-dioxo-6-thianaphthacen-2-carboxamid, racemat which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 70098-67-8,70116-55-1,82950-78-5
7-Dimethylamino-4-thiobenzamido-3,10,12-trihydroxy-1,4,4a,5,5a,6,11,12a-oktahydro-1,11-dioxo-6-thianaphthacen-2-carboxamid

: 70098-67-8,70116-55-1,82950-78-5
(+/-)-7-Dimethylamino-4-thiobenzamido-3,10,12-trihydroxy-1,4β,4aα,5,5aα,6,11,12aα-oktahydro-1,11-dioxo-6-thianaphthacen-2-carboxamid, racemat

Guidance literature:: With piperidine; at 50 ℃; for 3h; Yield given;
DOI:10.1002/ardp.19823150608

Reference yield:

: 22009-09-2
Acetondicarbonsaeuremethylestermonoamid

: 70098-64-5,82925-82-4
2-Phenyl-4<2-(8-dimethylamino-5-hydroxy-thiochroman-4-on-2-yl)-ethyliden>-2-thiazolin-5-on

: 70098-67-8,70116-55-1,82950-78-5
7-Dimethylamino-4-thiobenzamido-3,10,12-trihydroxy-1,4,4a,5,5a,6,11,12a-oktahydro-1,11-dioxo-6-thianaphthacen-2-carboxamid

Guidance literature:: With sodium hydride; Yield given. Multistep reaction; 1.) pyridine, 3 h, 2.) DMF, reflux, 2 h;
DOI:10.1002/ardp.19823150608

Reference yield: 42.0%

: 70098-67-8,70116-55-1,82950-78-5
(+/-)-7-Dimethylamino-4-thiobenzamido-3,10,12-trihydroxy-1,4β,4aα,5,5aα,6,11,12aα-oktahydro-1,11-dioxo-6-thianaphthacen-2-carboxamid, racemat

: 82925-83-5
(+/-)-7-Dimethylamino-3,10,12,12aα-tetrahydroxy-4-thiabenzamido-1,4β,4aα,5,5aα,6,11,12a-oktahydro-1,11-dioxo-6-thianaphthacen-2-carboxamid

Guidance literature:: With triethyl phosphate; potassium tert-butylate; oxygen; sodium methylate; In N,N-dimethyl-formamide; 1.) -14 deg C, 1 h, 2.) -2 deg C, 5 min;
DOI:10.1002/ardp.19823150608