2,6-(2,6-(i)Pr₂-C₆H₃N=CMe)2-4-CF₃-C₅H₂N

Base Information

Chemical Name:2,6-(2,6-(i)Pr₂-C₆H₃N=CMe)2-4-CF₃-C₅H₂N
CAS No.:210155-50-3
Molecular Formula:C₃₄H₄₂F₃N₃
Molecular Weight:549.723
Hs Code.:

2,6-(2,6-(i)Pr<sub>2</sub>-C<sub>6</sub>H<sub>3</sub>N=CMe)2-4-CF<sub>3</sub>-C<sub>5</sub>H<sub>2</sub>N

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Chemical Property of 2,6-(2,6-(i)Pr₂-C₆H₃N=CMe)2-4-CF₃-C₅H₂N

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Technology Process of 2,6-(2,6-(i)Pr₂-C₆H₃N=CMe)2-4-CF₃-C₅H₂N

There total 6 articles about 2,6-(2,6-(i)Pr₂-C₆H₃N=CMe)2-4-CF₃-C₅H₂N which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5371-70-0
dimethyl 4-chloro-2,6-pyridinedicarboxylate

: 210155-50-3
2,6-(2,6-(i)Pr₂-C₆H₃N=CMe)2-4-CF₃-C₅H₂N

Guidance literature:: Multi-step reaction with 4 steps

1.1: acetyl chloride; sodium iodide / acetonitrile

2.1: copper(l) iodide; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂ / N,N-dimethyl-formamide / 100 °C

3.1: sodium ethanolate / ethyl acetate / 7 h / Reflux

3.2: 12 h / Reflux

4.1: formic acid / methanol / 72 h / Reflux

With copper(l) iodide; formic acid; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; sodium ethanolate; acetyl chloride; sodium iodide; In methanol; ethyl acetate; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/om201212m

Reference yield:

: 112776-84-8
4-iodo-2,6-pyridinedicarboxylic acid dimethyl ester

: 210155-50-3
2,6-(2,6-(i)Pr₂-C₆H₃N=CMe)2-4-CF₃-C₅H₂N

Guidance literature:: Multi-step reaction with 3 steps

1.1: copper(l) iodide; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂ / N,N-dimethyl-formamide / 100 °C

2.1: sodium ethanolate / ethyl acetate / 7 h / Reflux

2.2: 12 h / Reflux

3.1: formic acid / methanol / 72 h / Reflux

With copper(l) iodide; formic acid; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; sodium ethanolate; In methanol; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1021/om201212m

Reference yield:

: 1009339-36-9
dimethyl 4-(trifluoromethyl)pyridine-2,6-dicarboxylate

: 210155-50-3
2,6-(2,6-(i)Pr₂-C₆H₃N=CMe)2-4-CF₃-C₅H₂N

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium ethanolate / ethyl acetate / 7 h / Reflux

1.2: 12 h / Reflux

2.1: formic acid / methanol / 72 h / Reflux

With formic acid; sodium ethanolate; In methanol; ethyl acetate;
DOI:10.1021/om201212m