[(3,4,5-F₃C₆H₂NCH₂CH₂)2NMe]TaCl₃

Base Information

Chemical Name:[(3,4,5-F₃C₆H₂NCH₂CH₂)2NMe]TaCl₃
CAS No.:919479-87-1
Molecular Formula:C₁₇H₁₅Cl₃F₆N₃Ta
Molecular Weight:662.624
Hs Code.:

[(3,4,5-F<sub>3</sub>C<sub>6</sub>H<sub>2</sub>NCH<sub>2</sub>CH<sub>2</sub>)2NMe]TaCl<sub>3</sub>

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Chemical Property of [(3,4,5-F₃C₆H₂NCH₂CH₂)2NMe]TaCl₃

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Technology Process of [(3,4,5-F₃C₆H₂NCH₂CH₂)2NMe]TaCl₃

There total 1 articles about [(3,4,5-F₃C₆H₂NCH₂CH₂)2NMe]TaCl₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 348630-65-9
H₂[(3,4,5-F₃C₆H₂NCH₂CH₂)2NMe]

: 7721-01-9
tantalum pentachloride

: 919479-87-1
[(3,4,5-F₃C₆H₂NCH₂CH₂)2NMe]TaCl₃

Guidance literature:: With (C₂H₅)3N; In dichloromethane; byproducts: [(C2H5)3NH]Cl; TaCl5 added to a soln. of ligand at -30°C, (C2H5)3N added, stirred for 5 h; evapd. (vac.), dissolved in THF, pptd. at -30°C for 15 min, filtered, concd. (vac.), collected on a frit, washed (pentane), dried (vac.);elem. anal.;
DOI:10.1016/j.ica.2006.03.044

Reference yield: 67.0%

: 919479-87-1
[(3,4,5-F₃C₆H₂NCH₂CH₂)2NMe]TaCl₃

: 13170-43-9
(trimethylsilyl)methylmagnesium chloride

: [(3,4,5-F₃C₆H₂NCH₂CH₂)2NMe]Ta(CHSiMe₃)(CH₂SiMe₃)

Guidance literature:: In diethyl ether; Mg compd. added dropwise to a suspn. of Ta complex at -30°C, reacted for 60 min, 1,4-dioxane added, stirred for 10 min, filtered, rinsed with ether, concd. (vac.), dissolved in toluene, heated to 50°C for 3 h; evapd. (vac.), triturated with pentane, filtered off, rinsed with pentane, dried (vac.); elem. anal.;
DOI:10.1016/j.ica.2006.03.044

Reference yield: 60.0%

: 919479-87-1
[(3,4,5-F₃C₆H₂NCH₂CH₂)2NMe]TaCl₃

: 676-58-4
methylmagnesium chloride

: 919479-88-2
[(3,4,5-F₃C₆H₂NCH₂CH₂)2NMe]TaMe₃

Guidance literature:: In tetrahydrofuran; diethyl ether; CH3MgCl in THF added to a suspn. of Ta complex in Et2O at -30°C, allowed to warm to room temp., reacted for 1 h; 1,4-dioxane added, filtered, concd. (vac.), rinsed with pentane, dried (vac.); elem. anal.;
DOI:10.1016/j.ica.2006.03.044