C₁₃H₁₃BrNP

Base Information

Chemical Name:C₁₃H₁₃BrNP
CAS No.:1263914-42-6
Molecular Formula:C₁₃H₁₃BrNP
Molecular Weight:294.131
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₃H₁₃BrNP

Chemical Property:

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Technology Process of C₁₃H₁₃BrNP

There total 4 articles about C₁₃H₁₃BrNP which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 20.0%

: 1263913-97-8
2-(2-bromobenzoylamido)phenylphosphonic acid diethyl ester

: 1263914-38-0
2-bromophenyl-1H-1,3benzazaphosphole

: 1263914-42-6
C₁₃H₁₃BrNP

: 67405-20-3
2-phenyl-1H-1,3-benzazaphosphole

Guidance literature:: With lithium aluminium tetrahydride; In diethyl ether; at 0 - 20 ℃; for 24h; Inert atmosphere;
DOI:10.1039/c0dt00881h

Reference yield:

: 7154-66-7
2-bromobenzoic acid chloride

: 1263914-38-0
2-bromophenyl-1H-1,3benzazaphosphole

: 1263914-42-6
C₁₃H₁₃BrNP

: 67405-20-3
2-phenyl-1H-1,3-benzazaphosphole

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / diethyl ether / 0 - 20 °C / Inert atmosphere

2: nickel dibromide / 0.33 h / 190 °C / Inert atmosphere

3: lithium aluminium tetrahydride / diethyl ether / 24 h / 0 - 20 °C / Inert atmosphere

With lithium aluminium tetrahydride; triethylamine; nickel dibromide; In diethyl ether;
DOI:10.1039/c0dt00881h

Reference yield:

: 2-bromo-N-(2-bromophenyl)-benzamide

: 1263914-38-0
2-bromophenyl-1H-1,3benzazaphosphole

: 1263914-42-6
C₁₃H₁₃BrNP

: 67405-20-3
2-phenyl-1H-1,3-benzazaphosphole

Guidance literature:: Multi-step reaction with 2 steps

1: nickel dibromide / 0.33 h / 190 °C / Inert atmosphere

2: lithium aluminium tetrahydride / diethyl ether / 24 h / 0 - 20 °C / Inert atmosphere

With lithium aluminium tetrahydride; nickel dibromide; In diethyl ether;
DOI:10.1039/c0dt00881h