ethyl 2-(1-acetylindolidone-3-yl-2)-3-aminocinnamate

Base Information

Chemical Name:ethyl 2-(1-acetylindolidone-3-yl-2)-3-aminocinnamate
CAS No.:132993-46-5
Molecular Formula:C₂₁H₂₀N₂O₄
Molecular Weight:364.401
Hs Code.:

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Chemical Property of ethyl 2-(1-acetylindolidone-3-yl-2)-3-aminocinnamate

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Technology Process of ethyl 2-(1-acetylindolidone-3-yl-2)-3-aminocinnamate

There total 2 articles about ethyl 2-(1-acetylindolidone-3-yl-2)-3-aminocinnamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 53256-19-2
ethyl (Z)-3-amino-3-phenylacrylate

: 132993-66-9
2?-bromo-N-acetylindoxyl

: 132993-46-5,132993-74-9
ethyl 2-(1-acetylindolidone-3-yl-2)-3-aminocinnamate

Guidance literature:: In benzene; 1.) reflux, 30 min, 2.) RT, 24 h;
DOI:10.1007/BF00766589

Reference yield:

: 16800-68-3
1-acetyl-2,3-dihydro-1H-indol-3-one

: 132993-46-5,132993-74-9
ethyl 2-(1-acetylindolidone-3-yl-2)-3-aminocinnamate

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / bromine / CH₂Cl₂ / 20 °C

2: 60 percent / benzene / 1.) reflux, 30 min, 2.) RT, 24 h

With bromine; In dichloromethane; benzene;
DOI:10.1007/BF00766589