1,2,3,4,5-pentafluoro-6-(2-nitroethyl)benzene

Base Information

Chemical Name:1,2,3,4,5-pentafluoro-6-(2-nitroethyl)benzene
CAS No.:1312540-59-2
Molecular Formula:C₈H₄F₅NO₂
Molecular Weight:241.117
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,2,3,4,5-pentafluoro-6-(2-nitroethyl)benzene

Chemical Property:

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Technology Process of 1,2,3,4,5-pentafluoro-6-(2-nitroethyl)benzene

There total 3 articles about 1,2,3,4,5-pentafluoro-6-(2-nitroethyl)benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 653-37-2
perfluorobenzaldehyde

: 1312540-59-2
1,2,3,4,5-pentafluoro-6-(2-nitroethyl)benzene

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydroxide / methanol; water / 0.92 h / -5 - 0 °C

2: methanesulfonyl chloride; triethylamine / dichloromethane / 1 h / -20 °C / Inert atmosphere

3: sodium tetrahydroborate; silica gel / chloroform; isopropyl alcohol / 15.5 h / Inert atmosphere

With sodium tetrahydroborate; silica gel; methanesulfonyl chloride; triethylamine; sodium hydroxide; In methanol; dichloromethane; chloroform; water; isopropyl alcohol;
DOI:10.1002/anie.201100260

Reference yield:

: 19282-52-1
2-nitro-1-(perfluorophenyl)ethanol

: 1312540-59-2
1,2,3,4,5-pentafluoro-6-(2-nitroethyl)benzene

Guidance literature:: Multi-step reaction with 2 steps

1: methanesulfonyl chloride; triethylamine / dichloromethane / 1 h / -20 °C / Inert atmosphere

2: sodium tetrahydroborate; silica gel / chloroform; isopropyl alcohol / 15.5 h / Inert atmosphere

With sodium tetrahydroborate; silica gel; methanesulfonyl chloride; triethylamine; In dichloromethane; chloroform; isopropyl alcohol;
DOI:10.1002/anie.201100260

Reference yield:

: 207605-39-8
(E)-1,2,3,4,5-pentafluoro-6-(2-nitrovinyl)benzene

: 1312540-59-2
1,2,3,4,5-pentafluoro-6-(2-nitroethyl)benzene

Guidance literature:: With sodium tetrahydroborate; silica gel; In chloroform; isopropyl alcohol; for 15.5h; Inert atmosphere;
DOI:10.1002/anie.201100260