{Fe(meso-5,10,15,20-tetrakis(o-pivalamidophenyl)porphyrinato)(1-methylimidazole)2}

Base Information

• Chemical Name: {Fe(meso-5,10,15,20-tetrakis(o-pivalamidophenyl)porphyrinato)(1-methylimidazole)2}
• CAS No.: 52275-89-5
• Molecular Formula: C₇₂H₇₆FeN₁₂O₄
• Molecular Weight: 1229.32

Synonyms:

Chemical Property of {Fe(meso-5,10,15,20-tetrakis(o-pivalamidophenyl)porphyrinato)(1-methylimidazole)2}

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of {Fe(meso-5,10,15,20-tetrakis(o-pivalamidophenyl)porphyrinato)(1-methylimidazole)2}

There total 1 articles about {Fe(meso-5,10,15,20-tetrakis(o-pivalamidophenyl)porphyrinato)(1-methylimidazole)2} which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-methyl-1H-imidazole (616-47-7) + chloroiron(III) meso-α,α,α,α-tetrakis(o-pivalamidophenyl)porphyrinate (105118-92-1,92078-42-7,87334-91-6,86107-94-0,87334-93-8,87334-92-7,104486-25-1) → {Fe(meso-5,10,15,20-tetrakis(o-pivalamidophenyl)porphyrinato)(1-methylimidazole)2} (52275-89-5,75557-96-9)

Guidance literature:

With sodium dithionite; In water; benzene; a benzene soln. of the porphyrin and a ligand adding to H2O, after carefully removal of O2 the flask filling with Ar, solid Na2S2O4 adding, stirring for 30 min (UV monitoring), treating with anhydrous Na2SO4, solidsfiltering off, hexane adding; identified by UV spectrum;

DOI:10.1021/ja00301a016

Reference yield:

{Fe(meso-5,10,15,20-tetrakis(o-pivalamidophenyl)porphyrinato)(1-methylimidazole)2} (52275-89-5,75557-96-9) → chloroiron(III) meso-α,α,α,α-tetrakis(o-pivalamidophenyl)porphyrinate (105118-92-1,92078-42-7,87334-91-6,86107-94-0,87334-93-8,87334-92-7,104486-25-1)

Guidance literature:

With hydrogenchloride; hydrogen; oxygen; In ethanol; toluene; a toluene-ethanol soln. of the initial complex was placed in the flask filled with Ar at 25°C, then Ar was replaced by flushing with H2-O2 mixt., a soln. containing HCl and colloidal Pt on polyvinylpyrrolidone satd. with H2-O2 was added; monitored by UV spectrum; Kinetics;

DOI:10.1021/ja00301a016

Reference yield:

1-methyl-1H-imidazole (616-47-7) + {Fe(meso-5,10,15,20-tetrakis(o-pivalamidophenyl)porphyrinato)(1-methylimidazole)2} (52275-89-5,75557-96-9) → (5,10,15,20-tetrakis(α,α,α,α-O-pivalamidophenyl)porphyrinato)iron(II)(1-methylimidazole)(O2) (55449-22-4,75559-87-4)

Guidance literature:

With hydrogen; oxygen; In ethanol; toluene; an aliquot of the diluted toluene soln. of the porphyrin and Me-imidazole was mixed with EtOH under Ar, then Ar was replaced by flushing with amixt. of H2-O2 gas; identified by UV spectrum;

DOI:10.1021/ja00301a016

upstream raw materials:

1-methyl-1H-imidazole

chloroiron(III) meso-α,α,α,α-tetrakis(o-pivalamidophenyl)porphyrinate

Downstream raw materials:

chloroiron(III) meso-α,α,α,α-tetrakis(o-pivalamidophenyl)porphyrinate

(5,10,15,20-tetrakis(α,α,α,α-O-pivalamidophenyl)porphyrinato)iron(II)(1-methylimidazole)(O2)

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