Na⁽¹⁺⁾*C₂B₉H₁₀C₆H₅Re(CO)3^(1-)=NaC₂B₉H₁₀C₆H₅Re(CO)3

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Chemical Name:Na⁽¹⁺⁾*C₂B₉H₁₀C₆H₅Re(CO)3^(1-)=NaC₂B₉H₁₀C₆H₅Re(CO)3
CAS No.:1023758-51-1
Molecular Formula:C₁₁H₁₅B₉O₃Re*Na
Molecular Weight:501.734
Hs Code.:

Na<sup>(1+)</sup>*C<sub>2</sub>B<sub>9</sub>H<sub>10</sub>C<sub>6</sub>H<sub>5</sub>Re(CO)3<sup>(1-)</sup>=NaC<sub>2</sub>B<sub>9</sub>H<sub>10</sub>C<sub>6</sub>H<sub>5</sub>Re(CO)3

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Chemical Property of Na⁽¹⁺⁾*C₂B₉H₁₀C₆H₅Re(CO)3^(1-)=NaC₂B₉H₁₀C₆H₅Re(CO)3

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Technology Process of Na⁽¹⁺⁾*C₂B₉H₁₀C₆H₅Re(CO)3^(1-)=NaC₂B₉H₁₀C₆H₅Re(CO)3

There total 1 articles about Na⁽¹⁺⁾*C₂B₉H₁₀C₆H₅Re(CO)3^(1-)=NaC₂B₉H₁₀C₆H₅Re(CO)3 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 159542-56-0,627528-38-5,912279-97-1
fac-triaquatricarbonylrhenium(I)

: Na⁽¹⁺⁾*C₂B₉H₁₁C₆H₅^(1-)=NaC₂B₉H₁₁C₆H₅

: 14333-24-5
perrhenate

: 1023758-51-1
Na⁽¹⁺⁾*C₂B₉H₁₀C₆H₅Re(CO)3^(1-)=NaC₂B₉H₁₀C₆H₅Re(CO)3

Guidance literature:: In not given; other Radiation; (Ar); addn. of a mixt. of (186/188)Re complexes to a soln. of boron compd., microwave heating for 5 min at 200°C; C18 solid phase extn. cartridge, flushing with H2O, elution with methanol, identified by radio-HPLC (Nucleosil C18 column, tetraethylammonium phosphate in methanol 100% to 0% 0-22 min, 0-100% 22-30 min);
DOI:10.1021/om8011807

Reference yield: 38.0%

: 1023758-51-1
Na⁽¹⁺⁾*C₂B₉H₁₀C₆H₅Re(CO)3^(1-)=NaC₂B₉H₁₀C₆H₅Re(CO)3

: 7664-93-9
sulfuric acid

: 7632-00-0
sodium nitrite

: 1153642-20-6
[2,2-(CO)2-2-(NO)-8-(Ph)-1,1,8-closo-ReC₂B₉H₁₀]

Guidance literature:: In water; addn. of aq. NaNO2 and H2SO4 to a soln. of (186/188)Re complex, react. for 5 min; C18 solid phase extn. carteidge, flushing with aq. acetonitrile 60%, then neat acetonitrile; identified by radio-HPLC (Nucleosil C18 column, 85-98% acetonitrile in H2O 0-17 min, 98% acetonitrile in H2O 17-20 min);
DOI:10.1021/om8011807