C₂₂H₂₂O₇

Base Information

Chemical Name:C₂₂H₂₂O₇
CAS No.:897954-00-6
Molecular Formula:C₂₂H₂₂O₇
Molecular Weight:398.412
Hs Code.:

C<sub>22</sub>H<sub>22</sub>O<sub>7</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₂H₂₂O₇

Chemical Property:

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Technology Process of C₂₂H₂₂O₇

There total 2 articles about C₂₂H₂₂O₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 96149-47-2
(1R,2R)-1,2-bis((R)-2,2-dimethyl-1,3-dioxolan-4-yl)ethane-1,2-diyl-dibenzoate

: 897954-00-6
C₂₂H₂₂O₇

Guidance literature:: With periodic acid; In diethyl ether; at 20 ℃; for 6h;
DOI:10.1016/j.tetasy.2009.10.030

Reference yield:

: 69-65-8
mannitol

: 897954-00-6
C₂₂H₂₂O₇

Guidance literature:: Multi-step reaction with 3 steps

1.1: toluene-4-sulfonic acid / dimethyl sulfoxide / 6 h / 20 °C

2.1: triethylamine / dichloromethane / 6 h / Inert atmosphere

3.1: periodic acid / diethyl ether / 6 h / 0 - 20 °C

3.2: 0.5 h

With toluene-4-sulfonic acid; periodic acid; triethylamine; In diethyl ether; dichloromethane; dimethyl sulfoxide;
DOI:10.1002/hlca.201100086

Reference yield:

: 897954-00-6
C₂₂H₂₂O₇

: 1779-49-3
Methyltriphenylphosphonium bromide

: 1357379-95-3
1,2-dideoxy-5,6-O-(1-methylethylidene)-D-arabino-hex-1-enitol 3,4-dibenzoate

Guidance literature:: Methyltriphenylphosphonium bromide; With potassium tert-butylate; In tetrahydrofuran; at -10 - 20 ℃; for 2h;

C₂₂H₂₂O₇; In tetrahydrofuran; at -10 ℃; for 2h;
DOI:10.1002/hlca.201100086