bromophenylacetaldehyde allyl ethyl acetal

Base Information

• Chemical Name: bromophenylacetaldehyde allyl ethyl acetal
• CAS No.: 110969-20-5
• Molecular Formula: C₁₂H₁₅BrO₂
• Molecular Weight: 271.154
• Mol file: 110969-20-5.mol

Synonyms:

Chemical Property of bromophenylacetaldehyde allyl ethyl acetal

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of bromophenylacetaldehyde allyl ethyl acetal

There total 1 articles about bromophenylacetaldehyde allyl ethyl acetal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

(E)-(2-methoxyvinyl)benzene (4110-75-2) + allyl alcohol (107-18-6) → bromophenylacetaldehyde allyl ethyl acetal (110969-20-5)

Guidance literature:

With N-Bromosuccinimide; at -50 - -20 ℃;

Reference yield:

bromophenylacetaldehyde allyl ethyl acetal (110969-20-5) → 3-methyl-2-phenyl-γ-butyrolactone + 3-methyl-2-phenyl-γ-butyrolactone (71018-33-2,99865-09-5,110969-25-0)

Guidance literature:

With sodium tetrahydroborate; jones reagent; tributyltin chloride; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts; 1.) benzene/ethanol, rt., irradiation; 2.) acetone/isopropyl alcohol, 0 deg C_.;

upstream raw materials:

(E)-(2-methoxyvinyl)benzene

allyl alcohol

Downstream raw materials:

3-methyl-2-phenyl-γ-butyrolactone