Fe2(mesityl)2(μ-S-2,6-dimesitylphenyl)(μ-mesityl)

Base Information

Chemical Name:Fe2(mesityl)2(μ-S-2,6-dimesitylphenyl)(μ-mesityl)
CAS No.:1234175-91-7
Molecular Formula:C₅₁H₅₈Fe₂S
Molecular Weight:814.782
Hs Code.:

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Chemical Property of Fe2(mesityl)2(μ-S-2,6-dimesitylphenyl)(μ-mesityl)

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Technology Process of Fe2(mesityl)2(μ-S-2,6-dimesitylphenyl)(μ-mesityl)

There total 2 articles about Fe2(mesityl)2(μ-S-2,6-dimesitylphenyl)(μ-mesityl) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 158100-80-2
Fe₂(mesityl)4

: 157590-41-5
2,2'',4,4'',6,6''-hexamethyl-[1,1':3',1''-terphenyl]-2'-thiol

: 1234175-91-7
Fe2(mesityl)2(μ-S-2,6-dimesitylphenyl)(μ-mesityl)

Guidance literature:: In diethyl ether; under N2 or Ar; Et2O soln. of ligand added slowly to Et2O soln. of Fe complex (molar ratio 1:1) at -80°C; gradually warmed to room temp.;stirred overnight; ppt. collected; washed with hexane; dried under vac.; elem. anal.;
DOI:10.1021/ic100692v

Reference yield:

: 158100-80-2
Fe₂(mesityl)4

: 157590-41-5
2,2'',4,4'',6,6''-hexamethyl-[1,1':3',1''-terphenyl]-2'-thiol

: Fe(S-2,6-dimesitylphenyl)2

: 1234175-91-7
Fe2(mesityl)2(μ-S-2,6-dimesitylphenyl)(μ-mesityl)

Guidance literature:: In diethyl ether; under N2 or Ar; Et2O soln. of ligand added slowly to Et2O soln. of Fe complex (molar ratio 2:1) at -80°C; gradually warmed to room temp.;stirred overnight;
DOI:10.1021/ic100692v