Technology Process of C7H3(2)H3O2
There total 4 articles about C7H3(2)H3O2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
deuteriated sodium hydroxide;
copper aluminum;
at 40 ℃;
for 0.5h;
Yield given;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: NaNO2, conc. H2SO4 / acetic acid / below 20 deg C, then 1 h, 30 deg C
2: CuBr, 36percent HBr / acetic acid / ice-water cooling, then 80 deg C
3: 1.) 5 percent NaOD-D2O, Cu-Al alloy, 2.) KMnO4 / 1.) addition gradually, 50 deg C, 140 min
With
potassium permanganate; deuteriated sodium hydroxide; copper aluminum; sulfuric acid; hydrogen bromide; copper(I) bromide; sodium nitrite;
In
acetic acid;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: CuBr, 36percent HBr / acetic acid / ice-water cooling, then 80 deg C
2: 1.) 5 percent NaOD-D2O, Cu-Al alloy, 2.) KMnO4 / 1.) addition gradually, 50 deg C, 140 min
With
potassium permanganate; deuteriated sodium hydroxide; copper aluminum; hydrogen bromide; copper(I) bromide;
In
acetic acid;