3,4,5-TRIBROMOACETOPHENONE

Base Information

Chemical Name:3,4,5-TRIBROMOACETOPHENONE
CAS No.:104892-58-2
Molecular Formula:C8H5Br3O
Molecular Weight:356.83700
Hs Code.:
Mol file:104892-58-2.mol

Synonyms:3,4,5-tribromoacetophenone;3.4.5-Tribrom-acetophenon;

Suppliers and Price of 3,4,5-TRIBROMOACETOPHENONE

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
3,4,5-Tribromoacetophenone
100mg
$ 65.00

Alichem
1-(3,4,5-Tribromophenyl)ethanone
25g
$ 3518.84

Alichem
1-(3,4,5-Tribromophenyl)ethanone
10g
$ 1989.90

Alichem
1-(3,4,5-Tribromophenyl)ethanone
5g
$ 1447.20

Total 2 raw suppliers

Chemical Property of 3,4,5-TRIBROMOACETOPHENONE

Chemical Property:

PSA：17.07000
LogP:4.17670

Purity/Quality:

95% ^*data from raw suppliers

3,4,5-Tribromoacetophenone ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 3,4,5-TRIBROMOACETOPHENONE

There total 6 articles about 3,4,5-TRIBROMOACETOPHENONE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 99-90-1
para-bromoacetophenone

: 3114-30-5
1-(3,4-dibromophenyl)ethan-1-one

: 104892-58-2
3,4,5-tribromoacetophenone

Guidance literature:: With bromine; aluminium trichloride; In 1,2-dichloro-ethane; at 20 ℃; for 72h;
DOI:10.1021/jo025822o

Reference yield:

: 4-Acetyl-2,6-dibromo-benzenediazonium; hydrogen sulfate

: 104892-58-2
3,4,5-tribromoacetophenone

Guidance literature:: With hydrogen bromide; copper(I) bromide; In acetic acid; Yield given; ice-water cooling, then 80 deg C;

Reference yield:

: 22589-50-0
4-amino-3,5-dibromo-acetophenone

: 104892-58-2
3,4,5-tribromoacetophenone

Guidance literature:: Multi-step reaction with 2 steps

1: NaNO₂, conc. H₂SO₄ / acetic acid / below 20 deg C, then 1 h, 30 deg C

2: CuBr, 36percent HBr / acetic acid / ice-water cooling, then 80 deg C

With sulfuric acid; hydrogen bromide; copper(I) bromide; sodium nitrite; In acetic acid;