Technology Process of C21H24N2O4
There total 1 articles about C21H24N2O4 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
3-methyl-N-phenyl-4-pyridinecarboxamide;
With
n-butyllithium;
In
tetrahydrofuran;
at -78 ℃;
cyclohexanedione monoethylene ketal;
at -78 - 23 ℃;
DOI:10.1016/j.bmcl.2012.02.098
- Guidance literature:
-
Multi-step reaction with 3 steps
1: sulfuric acid / water; acetic acid / 18 h / 65 °C
2: sodium tris(acetoxy)borohydride; triethylamine / 1,2-dichloro-ethane / 23 °C
3: dimethyl sulfoxide / 23 °C
With
sulfuric acid; sodium tris(acetoxy)borohydride; triethylamine;
In
water; acetic acid; dimethyl sulfoxide; 1,2-dichloro-ethane;
DOI:10.1016/j.bmcl.2012.02.098
- Guidance literature:
-
Multi-step reaction with 3 steps
1: sulfuric acid / water; acetic acid / 18 h / 65 °C
2: sodium tris(acetoxy)borohydride; triethylamine / 1,2-dichloro-ethane / 23 °C
3: dimethyl sulfoxide / 23 °C
With
sulfuric acid; sodium tris(acetoxy)borohydride; triethylamine;
In
water; acetic acid; dimethyl sulfoxide; 1,2-dichloro-ethane;
DOI:10.1016/j.bmcl.2012.02.098