(4R)-N,N-dibenzyl-4-((3R,5R,8R,9S,10S,12S,13R,17R)-3,12-bis(benzyloxy)-10,13-dimethylhexadecahydro-1H-cyclopenta[a]phenanthren-17-yl)-1,1-dimethoxypentan-2-amine

Base Information

Chemical Name:(4R)-N,N-dibenzyl-4-((3R,5R,8R,9S,10S,12S,13R,17R)-3,12-bis(benzyloxy)-10,13-dimethylhexadecahydro-1H-cyclopenta[a]phenanthren-17-yl)-1,1-dimethoxypentan-2-amine
CAS No.:1402067-80-4
Molecular Formula:C₅₄H₇₁NO₄
Molecular Weight:798.162
Hs Code.:

(4R)-N,N-dibenzyl-4-((3R,5R,8R,9S,10S,12S,13R,17R)-3,12-bis(benzyloxy)-10,13-dimethylhexadecahydro-1H-cyclopenta[a]phenanthren-17-yl)-1,1-dimethoxypentan-2-amine

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Chemical Property of (4R)-N,N-dibenzyl-4-((3R,5R,8R,9S,10S,12S,13R,17R)-3,12-bis(benzyloxy)-10,13-dimethylhexadecahydro-1H-cyclopenta[a]phenanthren-17-yl)-1,1-dimethoxypentan-2-amine

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Technology Process of (4R)-N,N-dibenzyl-4-((3R,5R,8R,9S,10S,12S,13R,17R)-3,12-bis(benzyloxy)-10,13-dimethylhexadecahydro-1H-cyclopenta[a]phenanthren-17-yl)-1,1-dimethoxypentan-2-amine

There total 3 articles about (4R)-N,N-dibenzyl-4-((3R,5R,8R,9S,10S,12S,13R,17R)-3,12-bis(benzyloxy)-10,13-dimethylhexadecahydro-1H-cyclopenta[a]phenanthren-17-yl)-1,1-dimethoxypentan-2-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 67-56-1
methanol

: 1402067-75-7
(4R)-4-((3R,5R,8R,9S,10S,12S,13R,17R)-3,12-bis(benzyloxy)-10,13-dimethylhexadecahydro-1H-cyclopenta[a]phenanthren-17-yl)pentanal

: 103-49-1
dibenzylamine

: 1402067-80-4
(4R)-N,N-dibenzyl-4-((3R,5R,8R,9S,10S,12S,13R,17R)-3,12-bis(benzyloxy)-10,13-dimethylhexadecahydro-1H-cyclopenta[a]phenanthren-17-yl)-1,1-dimethoxypentan-2-amine

: 1402067-73-5
C₅₄H₇₁NO₄

Guidance literature:: With sodium percarbonate; iodine; In dichloromethane; at 40 ℃; Overall yield = 85 %; Optical yield = 82 %de;
DOI:10.1002/anie.201204215

Reference yield:

: 83-44-3
Deoxycholic acid

: 1402067-80-4
(4R)-N,N-dibenzyl-4-((3R,5R,8R,9S,10S,12S,13R,17R)-3,12-bis(benzyloxy)-10,13-dimethylhexadecahydro-1H-cyclopenta[a]phenanthren-17-yl)-1,1-dimethoxypentan-2-amine

: 1402067-73-5
C₅₄H₇₁NO₄

Guidance literature:: Multi-step reaction with 4 steps

1: sulfuric acid / 20 °C

2: silver trifluoromethanesulfonate; 2,6-di-tert-butyl-pyridine / dichloromethane / 3 h / Reflux

3: lithium aluminium tetrahydride / tetrahydrofuran

4: iodine; sodium percarbonate / dichloromethane / 40 °C

With lithium aluminium tetrahydride; 2,6-di-tert-butyl-pyridine; sodium percarbonate; sulfuric acid; iodine; silver trifluoromethanesulfonate; In tetrahydrofuran; dichloromethane;
DOI:10.1002/anie.201204215

Reference yield:

: 3245-38-3
methyl deoxycholate

: 1402067-80-4
(4R)-N,N-dibenzyl-4-((3R,5R,8R,9S,10S,12S,13R,17R)-3,12-bis(benzyloxy)-10,13-dimethylhexadecahydro-1H-cyclopenta[a]phenanthren-17-yl)-1,1-dimethoxypentan-2-amine

: 1402067-73-5
C₅₄H₇₁NO₄

Guidance literature:: Multi-step reaction with 3 steps

1: silver trifluoromethanesulfonate; 2,6-di-tert-butyl-pyridine / dichloromethane / 3 h / Reflux

2: lithium aluminium tetrahydride / tetrahydrofuran

3: iodine; sodium percarbonate / dichloromethane / 40 °C

With lithium aluminium tetrahydride; 2,6-di-tert-butyl-pyridine; sodium percarbonate; iodine; silver trifluoromethanesulfonate; In tetrahydrofuran; dichloromethane;
DOI:10.1002/anie.201204215