Technology Process of C66H82I4O8
There total 5 articles about C66H82I4O8 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
C29H38Br2O3; 1,4-diiodo-2,5-dimethoxybenzene;
With
tributyl-amine; palladium diacetate; tris-(o-tolyl)phosphine;
In
toluene;
for 48h;
Inert atmosphere;
With
sodium iodide;
In
acetone;
Reflux;
DOI:10.1021/ja304986t
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: 18-crown-6 ether; potassium carbonate / acetone / 72 h / 75 °C
2.1: tributyl-amine; palladium diacetate; tris-(o-tolyl)phosphine / toluene / 24 h / 80 °C
3.1: tetrakis(triphenylphosphine) palladium(0) / toluene / 12 h / 100 °C / Inert atmosphere
4.1: tributyl-amine; palladium diacetate; tris-(o-tolyl)phosphine / toluene / 48 h / Inert atmosphere
4.2: Reflux
With
tetrakis(triphenylphosphine) palladium(0); 18-crown-6 ether; tributyl-amine; palladium diacetate; potassium carbonate; tris-(o-tolyl)phosphine;
In
acetone; toluene;
DOI:10.1021/ja304986t
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: tetrakis(triphenylphosphine) palladium(0) / toluene / 12 h / 100 °C / Inert atmosphere
2.1: tributyl-amine; palladium diacetate; tris-(o-tolyl)phosphine / toluene / 48 h / Inert atmosphere
2.2: Reflux
With
tetrakis(triphenylphosphine) palladium(0); tributyl-amine; palladium diacetate; tris-(o-tolyl)phosphine;
In
toluene;
DOI:10.1021/ja304986t
