Technology Process of C44H56ClNO4
There total 5 articles about C44H56ClNO4 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: acetic anhydride; dipyridinium dichromate / dichloromethane / Reflux
2: hydroxylamine hydrochloride; pyridine / 1 h / 80 °C
3: dicyclohexyl-carbodiimide / Reflux
With
pyridine; dipyridinium dichromate; hydroxylamine hydrochloride; acetic anhydride; dicyclohexyl-carbodiimide;
In
dichloromethane;
DOI:10.3390/molecules18033615
- Guidance literature:
-
Multi-step reaction with 4 steps
1: potassium carbonate / N,N-dimethyl-formamide / 4 h / 20 °C
2: acetic anhydride; dipyridinium dichromate / dichloromethane / Reflux
3: hydroxylamine hydrochloride; pyridine / 1 h / 80 °C
4: dicyclohexyl-carbodiimide / Reflux
With
pyridine; dipyridinium dichromate; hydroxylamine hydrochloride; acetic anhydride; potassium carbonate; dicyclohexyl-carbodiimide;
In
dichloromethane; N,N-dimethyl-formamide;
DOI:10.3390/molecules18033615