C₂₆H₂₁NO

Base Information

Chemical Name:C₂₆H₂₁NO
CAS No.:1426442-42-3
Molecular Formula:C₂₆H₂₁NO
Molecular Weight:363.459
Hs Code.:

Synonyms:

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Chemical Property of C₂₆H₂₁NO

Chemical Property:

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Technology Process of C₂₆H₂₁NO

There total 6 articles about C₂₆H₂₁NO which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 916518-57-5
5-(5,5-dimethyl-1,3,2-dioxaborinan-2-yl)-1-methyl-1H-indole

: 1426442-17-2
C₂₂H₂₂O₃

: 1426442-42-3
C₂₆H₂₁NO

: C₂₆H₂₁NO

Guidance literature:: With bis(1,5-cyclooctadiene)nickel⁽⁰⁾; potassium tert-butylate; N,N'-dimesityl-4,5-dihydro-1H-imidazolium tetrafluoroborate; In tetrahydrofuran; toluene; butan-1-ol; at 20 ℃; for 24h; Overall yield = 80 %; Overall yield = 58.5 mg; enantioselective reaction; Inert atmosphere;
DOI:10.1021/ja311783k

Reference yield:

: 1122-91-4
4-bromo-benzaldehyde

: 1426442-42-3
C₂₆H₂₁NO

: C₂₆H₂₁NO

Guidance literature:: Multi-step reaction with 4 steps

1.1: diethylzinc / toluene / 12 h / 60 °C / Inert atmosphere

1.2: 12 h / 20 °C / Inert atmosphere

2.1: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; tricyclohexylphosphine; potassium phosphate / 1,4-dioxane; water / 16 h / 95 °C / Inert atmosphere

3.1: sodium hydride / N,N-dimethyl-formamide / 1 h / 0 °C / Inert atmosphere

3.2: 3 h / 0 - 20 °C / Inert atmosphere

4.1: bis(1,5-cyclooctadiene)nickel⁽⁰⁾; N,N'-dimesityl-4,5-dihydro-1H-imidazolium tetrafluoroborate; potassium tert-butylate / toluene; tetrahydrofuran; butan-1-ol / 24 h / 20 °C / Inert atmosphere

With bis(1,5-cyclooctadiene)nickel⁽⁰⁾; potassium phosphate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; potassium tert-butylate; diethylzinc; sodium hydride; N,N'-dimesityl-4,5-dihydro-1H-imidazolium tetrafluoroborate; tricyclohexylphosphine; In tetrahydrofuran; 1,4-dioxane; water; N,N-dimethyl-formamide; toluene; butan-1-ol; 2.1: |Suzuki Coupling;
DOI:10.1021/ja311783k

Reference yield:

: 98-80-6
phenylboronic acid

: 1426442-42-3
C₂₆H₂₁NO

: C₂₆H₂₁NO

Guidance literature:: Multi-step reaction with 4 steps

1.1: diethylzinc / toluene / 12 h / 60 °C / Inert atmosphere

1.2: 12 h / 20 °C / Inert atmosphere

2.1: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; tricyclohexylphosphine; potassium phosphate / 1,4-dioxane; water / 16 h / 95 °C / Inert atmosphere

3.1: sodium hydride / N,N-dimethyl-formamide / 1 h / 0 °C / Inert atmosphere

3.2: 3 h / 0 - 20 °C / Inert atmosphere

4.1: bis(1,5-cyclooctadiene)nickel⁽⁰⁾; N,N'-dimesityl-4,5-dihydro-1H-imidazolium tetrafluoroborate; potassium tert-butylate / toluene; tetrahydrofuran; butan-1-ol / 24 h / 20 °C / Inert atmosphere

With bis(1,5-cyclooctadiene)nickel⁽⁰⁾; potassium phosphate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; potassium tert-butylate; diethylzinc; sodium hydride; N,N'-dimesityl-4,5-dihydro-1H-imidazolium tetrafluoroborate; tricyclohexylphosphine; In tetrahydrofuran; 1,4-dioxane; water; N,N-dimethyl-formamide; toluene; butan-1-ol; 2.1: |Suzuki Coupling;
DOI:10.1021/ja311783k