(CH₃)3Sn(C₁₇H₁₁ClNO₂S)*H₂O

Base Information

• Chemical Name: (CH₃)3Sn(C₁₇H₁₁ClNO₂S)*H₂O
• CAS No.: 244269-07-6
• Molecular Formula: C₂₀H₂₀ClNO₂SSn*H₂O
• Molecular Weight: 510.629
• Mol file: 244269-07-6.mol

Synonyms:

Chemical Property of (CH₃)3Sn(C₁₇H₁₁ClNO₂S)*H₂O

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of (CH₃)3Sn(C₁₇H₁₁ClNO₂S)*H₂O

There total 2 articles about (CH₃)3Sn(C₁₇H₁₁ClNO₂S)*H₂O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

fentiazac (18046-21-4) + trimethyltin(IV)chloride (1066-45-1) → (CH3)3Sn(C17H11ClNO2S)*H2O (244269-07-6)

Guidance literature:

With sodium ethanolate; In ethanol; byproducts: NaCl; N2; to 0.1 mole of C2H5ONa in EtOH 0.1 mole of organic acid added, refluxed for 3-4 h, cooled, 0.1 mole of Sn-comp. added with constant stirring, refluxed for 5-6 h, stored overnight at room temp.; filtered, solv. removed in vac., recrystd. from CH2Cl2, elem. anal.;

DOI:10.1081/SIM-120014856

Reference yield: 73.0%

fentiazac (18046-21-4) + trimethyltin(IV) hydroxide (56-24-6) → (CH3)3Sn(C17H11ClNO2S)*H2O (244269-07-6)

Guidance literature:

In toluene; byproducts: H2O; N2; organic acid and Sn-comp. (molar ratio 1:1) mixed, refluxed for 3-4 h, H2O removed using a Dean and Stark apparatus; solv. removed in vac., activated charcoal in CHCl3 added, filtered, concd., stored at -5°C, recrystd. from CH2Cl2, elem. anal.;

DOI:10.1081/SIM-120014856

upstream raw materials:

fentiazac

trimethyltin(IV)chloride

trimethyltin(IV) hydroxide